4-Bromo-3-nitrobenzamide

Base Information

Chemical Name:4-Bromo-3-nitrobenzamide
CAS No.:879-93-6
Molecular Formula:C7H5BrN2O3
Molecular Weight:245.032
Hs Code.:2924299090
DSSTox Substance ID:DTXSID20359320
Nikkaji Number:J851.938B
Wikidata:Q82140491
Mol file:879-93-6.mol

Synonyms:4-bromo-3-nitrobenzamide;879-93-6;DTXSID20359320;MFCD00462259;STK388462;AKOS003646362;SB77052;BS-25841;CS-0210281;A862340

Suppliers and Price of 4-Bromo-3-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-3-nitrobenzamide
100mg
$ 45.00

Matrix Scientific
4-Bromo-3-nitrobenzamide 95+%
5g
$ 773.00

Matrix Scientific
4-Bromo-3-nitrobenzamide 95+%
1g
$ 284.00

Crysdot
4-Bromo-3-nitrobenzamide 95+%
1g
$ 465.00

Alichem
4-Bromo-3-nitrobenzamide
1g
$ 1504.90

Alichem
4-Bromo-3-nitrobenzamide
500mg
$ 815.00

Alichem
4-Bromo-3-nitrobenzamide
250mg
$ 470.40

AK Scientific
4-Bromo-3-nitrobenzamide
5g
$ 291.00

Total 10 raw suppliers

Chemical Property of 4-Bromo-3-nitrobenzamide

Chemical Property:

Boiling Point:297.7±25.0 °C(Predicted)
PKA:14.58±0.50(Predicted)
PSA：88.91000
Density:1.799±0.06 g/cm3(Predicted)
LogP:2.67970
Storage Temp.:2-8°C
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:243.94835
Heavy Atom Count:13
Complexity:228

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-3-nitrobenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1C(=O)N)[N+](=O)[O-])Br

Technology Process of 4-Bromo-3-nitrobenzamide

There total 4 articles about 4-Bromo-3-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 335015-51-5
4-bromo-3-nitrobenzoyl chloride

: 879-93-6
4-bromo-3-nitrobenzamide

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran;

Reference yield: 74.0%

: 623-00-7
4-bromobenzenecarbonitrile

: 879-93-6
4-bromo-3-nitrobenzamide

Guidance literature:: With sulfuric acid; potassium nitrate; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c2cc30956d

Reference yield:

: 6319-40-0
4-bromo-3-nitrobenzoic acid

: 879-93-6
4-bromo-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / 85 °C

2: ammonium hydroxide / tetrahydrofuran / 2 h / 0 °C

With ammonium hydroxide; thionyl chloride; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2021.113554