Thieno[2,3-c]pyridin-2-amine, 4-(4-chlorophenyl)-4,5,6,7-tetrahydro-6-methyl-

Base Information

Chemical Name:Thieno[2,3-c]pyridin-2-amine, 4-(4-chlorophenyl)-4,5,6,7-tetrahydro-6-methyl-
CAS No.:88013-26-7
Molecular Formula:C14H15ClN2S
Molecular Weight:278.805
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Thieno[2,3-c]pyridin-2-amine, 4-(4-chlorophenyl)-4,5,6,7-tetrahydro-6-methyl-

Chemical Property:

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Technology Process of Thieno[2,3-c]pyridin-2-amine, 4-(4-chlorophenyl)-4,5,6,7-tetrahydro-6-methyl-

There total 7 articles about Thieno[2,3-c]pyridin-2-amine, 4-(4-chlorophenyl)-4,5,6,7-tetrahydro-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88013-64-3
4-p-chlorophenyl-6-methyl-2-nitro-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine

: 88013-26-7
2-amino-4-(4-chlorophenyl)-6-methyl-4,5,6,7-tetrahydrothieno<2,3-c>pyridine

Guidance literature:: With hydrogen; platinum on activated charcoal; at 25 ℃; for 2h; under 3750.3 Torr;
DOI:10.1021/jm00375a011

Reference yield:

: 58255-18-8
N-methyl-1-(thiophen-2-yl)methanamine

: 88013-26-7
2-amino-4-(4-chlorophenyl)-6-methyl-4,5,6,7-tetrahydrothieno<2,3-c>pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / ethanol

2: NaBH₄

3: 73 percent / methanesulfonic acid / 0.5 h / 70 °C

4: 85 percent / HNO₃ / trifluoroacetic acid / 1 h

5: H₂ / 5percent Pt on charcoal / 2 h / 25 °C / 3750.3 Torr

With sodium tetrahydroborate; methanesulfonic acid; hydrogen; nitric acid; potassium carbonate; platinum on activated charcoal; In ethanol; trifluoroacetic acid;
DOI:10.1021/jm00375a011

Reference yield:

: 70696-54-7
4-(4-chlorophenyl)-6-methyl-4,5,6,7-tetrahydrothieno<2,3-c>pyridine

: 88013-26-7
2-amino-4-(4-chlorophenyl)-6-methyl-4,5,6,7-tetrahydrothieno<2,3-c>pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / HNO₃ / trifluoroacetic acid / 1 h

2: H₂ / 5percent Pt on charcoal / 2 h / 25 °C / 3750.3 Torr

With hydrogen; nitric acid; platinum on activated charcoal; In trifluoroacetic acid;
DOI:10.1021/jm00375a011