Pentanoic acid, 4-oxo-, 9,9-bis[(benzoyloxy)methyl]-19,19-bis(4-methoxyphenyl)-6,12-dioxo-19- phenyl-7,11,18-trioxa-5,13-diazanonadec-1-yl ester

Base Information

• Chemical Name: Pentanoic acid, 4-oxo-, 9,9-bis[(benzoyloxy)methyl]-19,19-bis(4-methoxyphenyl)-6,12-dioxo-19- phenyl-7,11,18-trioxa-5,13-diazanonadec-1-yl ester
• CAS No.: 880145-69-7
• Molecular Formula: C55H62N2O14
• Molecular Weight: 975.102

Synonyms:

Chemical Property of Pentanoic acid, 4-oxo-, 9,9-bis[(benzoyloxy)methyl]-19,19-bis(4-methoxyphenyl)-6,12-dioxo-19- phenyl-7,11,18-trioxa-5,13-diazanonadec-1-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pentanoic acid, 4-oxo-, 9,9-bis[(benzoyloxy)methyl]-19,19-bis(4-methoxyphenyl)-6,12-dioxo-19- phenyl-7,11,18-trioxa-5,13-diazanonadec-1-yl ester

There total 1 articles about Pentanoic acid, 4-oxo-, 9,9-bis[(benzoyloxy)methyl]-19,19-bis(4-methoxyphenyl)-6,12-dioxo-19- phenyl-7,11,18-trioxa-5,13-diazanonadec-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-oxo-pentanoic acid 4-(3-{4-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-butylcarbamoyloxy}-2,2-bis-hydroxymethyl-propoxycarbonylamino)-butyl ester + benzoyl chloride (98-88-4) → benzoic acid 3-{4-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-butylcarbamoyloxy}-2-hydroxymethyl-2-[4-(4-oxo-pentanoyloxy)-butylcarbamoyloxymethyl]-propyl ester + C55H62N2O14 (880145-69-7)

Guidance literature:

With pyridine; at 20 ℃;

DOI:10.1016/j.bmcl.2005.11.036

Reference yield: 81.0%

C55H62N2O14 (880145-69-7) → C50H56N2O12 (880145-70-0)

Guidance literature:

With pyridine; hydrazine hydrate; acetic acid; at 20 ℃;

DOI:10.1016/j.bmcl.2005.11.036

Reference yield:

C55H62N2O14 (880145-69-7) → C59H73N4O13P

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / NH₂NH₂*H₂O; CH₃CO₂H; pyridine / 20 °C

2: 94 percent / EtN(iPr)2 / CH₂Cl₂ / 20 °C

With pyridine; hydrazine hydrate; acetic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1016/j.bmcl.2005.11.036

upstream raw materials:

benzoyl chloride

Downstream raw materials:

C₅₀H₅₆N₂O₁₂

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