(3β)-Yohimban

Base Information

Chemical Name:(3β)-Yohimban
CAS No.:7363-24-8
Molecular Formula:C19H24N2
Molecular Weight:280.40726
Hs Code.:
Mol file:7363-24-8.mol

Synonyms:yohimbane;epiyohimban;pseudo-yohimbane;3β-Yohimban;pseudo-Yohimban;(4aR,13bR,14aS)-1,2,3,4,4a,5,7,8,13,13b,14,14a-Dodecahydro-indolo[2',3':3,4]pyrido[1,2-b]isoquinoline;

Suppliers and Price of (3β)-Yohimban

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (3β)-Yohimban

Chemical Property:

PSA：19.03000
LogP:4.21510

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3β)-Yohimban

There total 28 articles about (3β)-Yohimban which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 128637-96-7
(4aR,13bS,14aR)-1,3,4,4a,5,7,8,13b,14,14a-Decahydro-2H-indolo[2',3':3,4]pyrido[1,2-b]isoquinoline-13-carboxylic acid tert-butyl ester

: 483-25-0,483-26-1,523-06-8,4695-98-1,7363-24-8,10283-60-0,14210-12-9,69349-93-5,133160-32-4
dl-Epialloyohimbane

Guidance literature:: In formic acid; for 70h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85442-9

Reference yield:

: 140192-37-6
(+/-)-1-allyl-2-(2-oxo-2H-pyran-6-ylcarbonyl)-1,2,3,4-tetrahydro-β-carboline

: 483-25-0,483-26-1,523-06-8,4695-98-1,7363-24-8,10283-60-0,14210-12-9,69349-93-5,133160-32-4
(+/-)-pseudo-yohimbane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / toluene / 42 h / Heating

2: 1.) H₂, 2.) LiAlH₄ / 1.) PtO₂ / 1.) MeOH, 2.) THF, reflux, 3.5 h

With lithium aluminium tetrahydride; hydrogen; platinum(IV) oxide; In toluene;
DOI:10.1246/bcsj.65.298

Reference yield:

: 140192-37-6
(+/-)-1-allyl-2-(2-oxo-2H-pyran-6-ylcarbonyl)-1,2,3,4-tetrahydro-β-carboline

: 483-25-0,483-26-1,523-06-8,4695-98-1,7363-24-8,10283-60-0,14210-12-9,69349-93-5,133160-32-4
dl-Epialloyohimbane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / toluene / 42 h / Heating

2: 1.) H₂, 2.) LiAlH₄ / 1.) PtO₂ / 1.) MeOH, 2.) THF, reflux, 3.5 h

With lithium aluminium tetrahydride; hydrogen; platinum(IV) oxide; In toluene;
DOI:10.1246/bcsj.65.298