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Propanoic acid, 3-[[4-(2-phenylethenyl)phenyl]thio]-, 2-ethylhexyl ester

Base Information Edit
  • Chemical Name:Propanoic acid, 3-[[4-(2-phenylethenyl)phenyl]thio]-, 2-ethylhexyl ester
  • CAS No.:881664-13-7
  • Molecular Formula:C25H32O2S
  • Molecular Weight:396.594
  • Hs Code.:
  • Mol file:881664-13-7.mol
Propanoic acid, 3-[[4-(2-phenylethenyl)phenyl]thio]-, 2-ethylhexyl ester

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Chemical Property of Propanoic acid, 3-[[4-(2-phenylethenyl)phenyl]thio]-, 2-ethylhexyl ester Edit
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Technology Process of Propanoic acid, 3-[[4-(2-phenylethenyl)phenyl]thio]-, 2-ethylhexyl ester

There total 5 articles about Propanoic acid, 3-[[4-(2-phenylethenyl)phenyl]thio]-, 2-ethylhexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 1-methyl-pyrrolidin-2-one; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine; at 130 ℃; for 10h;
DOI:10.1021/jo052624z
Guidance literature:
Multi-step reaction with 3 steps
1: 44.3 percent / copper / 4 h / 150 - 175 °C
2: 48.5 percent / triethylphosphite / 20 h / 165 °C
3: 30.6 percent / N,N-dimethyl-acetamide / 18 h / Heating
With copper; triethyl phosphite; In N,N-dimethyl acetamide; 1: Ullmann reaction;
DOI:10.1128/AAC.46.3.797-807.2002
Guidance literature:
Multi-step reaction with 2 steps
1: 93 percent / TBAF / tetrahydrofuran / 15 h / 20 °C
2: 92 percent / i-Pr2NEt; NMP; Pd(PPh3)4 / 10 h / 130 °C
With 1-methyl-pyrrolidin-2-one; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 2: Heck reaction;
DOI:10.1021/jo052624z
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