Methanol, (1,2-ethanediylbis(nitroimino))bis-, diacetate (ester)

Base Information

• Chemical Name: Methanol, (1,2-ethanediylbis(nitroimino))bis-, diacetate (ester)
• CAS No.: 14168-48-0
• Molecular Formula: C₈H₁₄N₄O₈
• Molecular Weight: 294.221
• DSSTox Substance ID: DTXSID40161801
• Wikidata: Q83030250
• Mol file: 14168-48-0.mol

Synonyms:BRN 1808347;Methanol, (1,2-ethanediylbis(nitroimino))bis-, diacetate (ester);14168-48-0;Methanol, ethylenebis(nitroimino)di-, diacetate (ester);(1,2-Ethanediylbis(nitroimino)bismethanol) diacetate (ester);3-04-00-00546 (Beilstein Handbook Reference);DTXSID40161801;LS-91028

Chemical Property of Methanol, (1,2-ethanediylbis(nitroimino))bis-, diacetate (ester)

Chemical Property:

• Vapor Pressure: 1.49E-11mmHg at 25°C
• Boiling Point: 535.8°Cat760mmHg
• Flash Point: 277.8°C
• Density: 1.417g/cm³
• XLogP3: 1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 9
• Exact Mass: 294.08116342
• Heavy Atom Count: 20
• Complexity: 340

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCN(CCN(COC(=O)C)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of Methanol, (1,2-ethanediylbis(nitroimino))bis-, diacetate (ester)

There total 5 articles about Methanol, (1,2-ethanediylbis(nitroimino))bis-, diacetate (ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-dinitro-1,4-diazabutane (505-71-5) + sodium acetate (127-09-3) + acetic anhydride (108-24-7) → 2,5-dinitro-2,5-diaza-1,6-hexanediyl diacetate (14168-48-0)

Guidance literature:

at 65 ℃;

Reference yield:

N,N'-dinitro-N,N'-bis-nitryloxymethyl-ethylenediamine (13126-27-7) + sodium acetate (127-09-3) + acetic acid (64-19-7,77671-22-8) → 2,5-dinitro-2,5-diaza-1,6-hexanediyl diacetate (14168-48-0)

Guidance literature:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1,4-dinitro-1,4-diazabutane (505-71-5) + acetic anhydride (108-24-7) → 2,5-dinitro-2,5-diaza-1,6-hexanediyl diacetate (14168-48-0)

Guidance literature:

Multistep reaction; (i) H₂O, (ii) /BRN= 385737/, Py;

upstream raw materials:

1,4-dinitro-1,4-diazabutane

sodium acetate

acetic anhydride

N,N'-dinitro-N,N'-bis-nitryloxymethyl-ethylenediamine