Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[2-nitro-

Base Information

Chemical Name:Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[2-nitro-
CAS No.:881693-47-6
Molecular Formula:C25H29N5O8S2
Molecular Weight:591.666
Hs Code.:

Synonyms:

Suppliers and Price of Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[2-nitro-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[2-nitro-

Chemical Property:

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Technology Process of Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[2-nitro-

There total 4 articles about Benzenesulfonamide, N,N'-[[(phenylmethyl)imino]di-3,1-propanediyl]bis[2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-94-4
3,3'-Iminodipropionitrile

: 881693-47-6
N,N'-bis(o-nitrobenzenesulfonyl)bis(3-aminopropyl)benzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaI; Na₂CO₃ / acetonitrile / 5 h / Heating

2: 81 percent / aq. NaOH; H₂ / Raney Ni / ethanol / 48 h / 1034.3 - 1551.44 Torr

3: aq. NaOH; NaCl / diethyl ether / 20 °C

With sodium hydroxide; hydrogen; sodium carbonate; sodium iodide; sodium chloride; nickel; In diethyl ether; ethanol; acetonitrile; 3: Schotten-Bauman sulfonylation;
DOI:10.1021/jm0582524

Reference yield:

: 782-87-6
N-benzylbis(2-cyanoethyl)amine

: 881693-47-6
N,N'-bis(o-nitrobenzenesulfonyl)bis(3-aminopropyl)benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / aq. NaOH; H₂ / Raney Ni / ethanol / 48 h / 1034.3 - 1551.44 Torr

2: aq. NaOH; NaCl / diethyl ether / 20 °C

With sodium hydroxide; hydrogen; sodium chloride; nickel; In diethyl ether; ethanol; 2: Schotten-Bauman sulfonylation;
DOI:10.1021/jm0582524

Reference yield:

: 100-44-7
benzyl chloride

: 881693-47-6
N,N'-bis(o-nitrobenzenesulfonyl)bis(3-aminopropyl)benzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaI; Na₂CO₃ / acetonitrile / 5 h / Heating

2: 81 percent / aq. NaOH; H₂ / Raney Ni / ethanol / 48 h / 1034.3 - 1551.44 Torr

3: aq. NaOH; NaCl / diethyl ether / 20 °C

With sodium hydroxide; hydrogen; sodium carbonate; sodium iodide; sodium chloride; nickel; In diethyl ether; ethanol; acetonitrile; 3: Schotten-Bauman sulfonylation;
DOI:10.1021/jm0582524