Benzeneacetamide, N-[(1S)-3-hydroxy-1-phenylpropyl]-

Base Information

Chemical Name:Benzeneacetamide, N-[(1S)-3-hydroxy-1-phenylpropyl]-
CAS No.:881853-41-4
Molecular Formula:C17H19NO2
Molecular Weight:269.343
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneacetamide, N-[(1S)-3-hydroxy-1-phenylpropyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzeneacetamide, N-[(1S)-3-hydroxy-1-phenylpropyl]-

There total 4 articles about Benzeneacetamide, N-[(1S)-3-hydroxy-1-phenylpropyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.5%

: 406468-05-1
3-[N-(phenylacetyl)amino]-3-phenyl-1-propanol

: 170564-98-4
(R)-3-amino-3-phenyl-1-propanol

: 881853-41-4
3-[N-(phenylacetyl)amino]-3-phenyl-1-propanol

Guidance literature:: With phosphate buffer; penicillin G acylase immobilized on epoxy-resin; In ethanol; water; at 25 ℃; for 1h; pH=7.5;
DOI:10.1016/j.tetasy.2005.12.022

Reference yield:

: 5650-41-9
3-hydroxy-1-phenylpropan-1-one

: 881853-41-4
3-[N-(phenylacetyl)amino]-3-phenyl-1-propanol

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / ammonium acetate; sodium cyanoborohydride / ethanol / 36 h / 20 °C

2: 80 percent / aq. NaOH / 4 h / 20 °C

3: 47.5 percent / penicillin G acylase immobilized on epoxy-resin; phosphate buffer / ethanol; H₂O / 1 h / 25 °C / pH 7.5

With ammonium acetate; sodium hydroxide; phosphate buffer; penicillin G acylase immobilized on epoxy-resin; sodium cyanoborohydride; In ethanol; water; 2: Schotten-Baumann reaction;
DOI:10.1016/j.tetasy.2005.12.022

Reference yield:

: 6296-54-4
ethyl 2,4-dioxo-4-phenylbutyrate

: 881853-41-4
3-[N-(phenylacetyl)amino]-3-phenyl-1-propanol

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Saccharomyces cerevisiae; glucose; phenacyl chloride / aq. phosphate buffer; diisopropyl ether / 48 h / 20 °C / pH 4.5

2: 65 percent / ammonium acetate; sodium cyanoborohydride / ethanol / 36 h / 20 °C

3: 80 percent / aq. NaOH / 4 h / 20 °C

4: 47.5 percent / penicillin G acylase immobilized on epoxy-resin; phosphate buffer / ethanol; H₂O / 1 h / 25 °C / pH 7.5

With Saccharomyces cerevisiae; ammonium acetate; sodium hydroxide; phosphate buffer; D-glucose; penicillin G acylase immobilized on epoxy-resin; sodium cyanoborohydride; 1-chloroacetophenone; In phosphate buffer; ethanol; di-isopropyl ether; water; 3: Schotten-Baumann reaction;
DOI:10.1016/j.tetasy.2005.12.022