4-chloro-2-[dichloro(phenyl)methyl]phenyl phosphorodichloridate

Base Information

• Chemical Name: 4-chloro-2-[dichloro(phenyl)methyl]phenyl phosphorodichloridate
• CAS No.: 5995-76-6
• Molecular Formula: C13H8 Cl5 O2 P
• Molecular Weight: 404.444

Synonyms:Phosphorodichloridicacid, a,a,4-trichloro-a-phenyl-o-tolyl ester (8CI); o-Cresol, a,a,4-trichloro-a-phenyl-, phosphorodichloridate (7CI);4-Chloro-2-[dichloro(phenyl)methyl]phenyl phosphorodichloridate; NSC 86398

Chemical Property of 4-chloro-2-[dichloro(phenyl)methyl]phenyl phosphorodichloridate

Chemical Property:

• Vapor Pressure: 5.51E-08mmHg at 25°C
• Boiling Point: 453.5°Cat760mmHg
• Flash Point: 372.7°C
• Density: 1.562g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chloro-2-[dichloro(phenyl)methyl]phenyl phosphorodichloridate

There total 3 articles about 4-chloro-2-[dichloro(phenyl)methyl]phenyl phosphorodichloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(5-chloro-2-hydroxyphenyl)phenylmethanone (85-19-8) → 4-chloro-2-(α,α-dichlorobenzyl)phenyl phosphochloridate (5995-76-6)

Guidance literature:

With phosphorus pentachloride;

DOI:10.1080/00304940409355397

Reference yield:

2-benzoyl-4-chlorophenylphosphorodichloridate (5995-77-7) → 4-chloro-2-(α,α-dichlorobenzyl)phenyl phosphochloridate (5995-76-6)

Guidance literature:

With phosphorus pentachloride; at 129 - 131 ℃; for 3h;

DOI:10.1080/00304940409355978

Reference yield:

→ 4-chloro-2-(α,α-dichlorobenzyl)phenyl phosphochloridate (5995-76-6)

Guidance literature:

5-Chlor-2-hydroxy-benzophenon, PCl5 in Bzl.;

upstream raw materials:

(5-chloro-2-hydroxyphenyl)phenylmethanone

2-benzoyl-4-chlorophenylphosphorodichloridate

Downstream raw materials:

(2,5-dichlorophenyl)(phenyl)methanone

4-chloro-2-(α,α-dichlorobenzyl)phenyldiphenyl phosphate

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