Thiazole, 4-(iodomethyl)-2-(4-methylphenyl)-

Base Information

Chemical Name:Thiazole, 4-(iodomethyl)-2-(4-methylphenyl)-
CAS No.:89152-41-0
Molecular Formula:C11H10INS
Molecular Weight:315.178
Hs Code.:

Synonyms:

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Chemical Property of Thiazole, 4-(iodomethyl)-2-(4-methylphenyl)-

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Technology Process of Thiazole, 4-(iodomethyl)-2-(4-methylphenyl)-

There total 2 articles about Thiazole, 4-(iodomethyl)-2-(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 35199-18-9
4-chloromethyl-2-(4-methyl-phenyl)-thiazole

: 89152-41-0
4-(iodomethyl)-2-(p-tolyl)thiazole

Guidance literature:: With sodium iodide; for 1h; Reflux;
DOI:10.1002/ejoc.201501495

Reference yield:

: 2362-62-1
4-methylthiobenzamide

: 89152-41-0
4-(iodomethyl)-2-(p-tolyl)thiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetone / 24 h / 20 °C

1.2: 3 h / 20 °C

2.1: sodium iodide / 1 h / Reflux

With sodium iodide; In acetone; 1.1: |Hantzsch Thiazole Synthesis / 1.2: |Hantzsch Thiazole Synthesis;
DOI:10.1002/ejoc.201501495

Reference yield: 57.0%

: 136520-15-5
1,1-dimethylethyl N-[(1R,2R,5R)-2-hydroxy-2,6,6-trimethylbicyclo[3.1.1]hept-3-ylidene]glycinate

: 89152-41-0
4-(iodomethyl)-2-(p-tolyl)thiazole

: C₂₇H₃₆N₂O₃S

Guidance literature:: 1,1-dimethylethyl N-[(1R,2R,5R)-2-hydroxy-2,6,6-trimethylbicyclo[3.1.1]hept-3-ylidene]glycinate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

4-(iodomethyl)-2-(p-tolyl)thiazole; In tetrahydrofuran; hexane; at -78 - -10 ℃; for 14h; diastereoselective reaction;
DOI:10.1002/ejoc.201501495