4-Piperidinone, 3-bromo-1-methyl-, hydrobromide

Base Information

Chemical Name:4-Piperidinone, 3-bromo-1-methyl-, hydrobromide
CAS No.:89580-42-7
Molecular Formula:C6H10BrNO.BrH
Molecular Weight:272.967
Hs Code.:
DSSTox Substance ID:DTXSID90597530
Mol file:89580-42-7.mol

Synonyms:89580-42-7;4-Piperidinone, 3-bromo-1-methyl-, hydrobromide;3-bromo-1-methylpiperidin-4-one;hydrobromide;SCHEMBL8843008;DTXSID90597530;DB-339167;3-BROMO-1-METHYLPIPERIDIN-4-ONE HBR;3-Bromo-1-Methyl-4-Piperidinone Hydrobromide;3-BROMO-1-METHYLPIPERIDIN-4-ONE HYDROBROMIDE;3-Bromo-1-methylpiperidin-4-one--hydrogen bromide (1/1)

Suppliers and Price of 4-Piperidinone, 3-bromo-1-methyl-, hydrobromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 4-Piperidinone, 3-bromo-1-methyl-, hydrobromide

Chemical Property:

Melting Point:120-122℃
PSA：20.31000
LogP:1.55050
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:272.91869
Heavy Atom Count:10
Complexity:126

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCC(=O)C(C1)Br.Br

Technology Process of 4-Piperidinone, 3-bromo-1-methyl-, hydrobromide

There total 1 articles about 4-Piperidinone, 3-bromo-1-methyl-, hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

: 1445-73-4
1-Methyl-4-piperidone

: 89580-42-7
3-bromo-1-methylpiperidin-4-one hydrobromide

Guidance literature:: With hydrogen bromide; bromine; acetic acid; In water; at 20 - 25 ℃; Large scale;

Reference yield: 9.3%

: 89580-42-7
3-bromo-1-methylpiperidin-4-one hydrobromide

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 645-54-5
2-phenylthioacetamide

: 2-benzyl-5-methyl-4,5,6,7-tetrahydrothiazole[5,4-c]pyridine fumarate

Guidance literature:: 3-bromo-1-methylpiperidin-4-one hydrobromide; 2-phenylthioacetamide; With calcium carbonate; In isopropyl alcohol; for 10h; Heating;

(2E)-but-2-enedioic acid; In methanol;
DOI:10.1016/S0968-0896(02)00557-6

Reference yield:

: 89580-42-7
3-bromo-1-methylpiperidin-4-one hydrobromide

: 143150-92-9
2-Bromo-5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]-pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 75 - 80 °C

2: hydrogen bromide; sodium nitrite / water / 3 h / 10 - 25 °C

With hydrogen bromide; sodium nitrite; In ethanol; water;