1-(4-Iodo-2,5-dimethoxyphenyl)propan-2-one

Base Information

Chemical Name:1-(4-Iodo-2,5-dimethoxyphenyl)propan-2-one
CAS No.:90064-49-6
Molecular Formula:C₁₁H₁₃IO₃
Molecular Weight:320.127
Hs Code.:
ChEMBL ID:CHEMBL2068770
DSSTox Substance ID:DTXSID70603668
Wikidata:Q82501145

Synonyms:90064-49-6;1-(4-Iodo-2,5-dimethoxyphenyl)propan-2-one;CHEMBL2068770;SCHEMBL10779495;DTXSID70603668

Suppliers and Price of 1-(4-Iodo-2,5-dimethoxyphenyl)propan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(4-Iodo-2,5-dimethoxyphenyl)propan-2-one

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:319.99094
Heavy Atom Count:15
Complexity:220

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)CC1=CC(=C(C=C1OC)I)OC

Technology Process of 1-(4-Iodo-2,5-dimethoxyphenyl)propan-2-one

There total 3 articles about 1-(4-Iodo-2,5-dimethoxyphenyl)propan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 90064-44-1
1-(4-iodo-2,5-dimethoxyphenyl)-2-nitropropene

: 90064-49-6
1-(4-iodo-2,5-dimethoxyphenyl)-2-propanone

Guidance literature:: With iron; acetic acid; for 0.5h; Heating;
DOI:10.1021/jm00374a023

Reference yield:

: 51560-21-5
1,4-diiodo-2,5-dimethoxybenzene

: 90064-49-6
1-(4-iodo-2,5-dimethoxyphenyl)-2-propanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) ether, hexane, 10 min, 2.) ether, hexane, a) RT, 10 min, b) reflux, 10 min

2: 40 percent / ammonium acetate / 6 h / Heating

3: 52 percent / electrolytic Fe, AcOH / 0.5 h / Heating

With ammonium acetate; n-butyllithium; iron; acetic acid;
DOI:10.1021/jm00374a023

Reference yield:

: 90064-47-4
4-iodo-2,5-dimethoxybenzenecarbaldehyde

: 90064-49-6
1-(4-iodo-2,5-dimethoxyphenyl)-2-propanone

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / ammonium acetate / 6 h / Heating

2: 52 percent / electrolytic Fe, AcOH / 0.5 h / Heating

With ammonium acetate; iron; acetic acid;
DOI:10.1021/jm00374a023