Dimethyl 4-acetyl-5-hydroxyphthalate

Base Information

Chemical Name:Dimethyl 4-acetyl-5-hydroxyphthalate
CAS No.:90330-50-0
Molecular Formula:C₁₂H₁₂O₆
Molecular Weight:252.224
Hs Code.:
DSSTox Substance ID:DTXSID101334057

Synonyms:dimethyl 4-acetyl-5-hydroxyphthalate;90330-50-0;SCHEMBL7862662;YEECPQAAZZPVNC-UHFFFAOYSA-N;DTXSID101334057

Suppliers and Price of Dimethyl 4-acetyl-5-hydroxyphthalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl 4-acetyl-5-hydroxyphthalate

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:252.06338810
Heavy Atom Count:18
Complexity:351

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=C(C=C(C(=C1)C(=O)OC)C(=O)OC)O

Technology Process of Dimethyl 4-acetyl-5-hydroxyphthalate

There total 3 articles about Dimethyl 4-acetyl-5-hydroxyphthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 90330-49-7
3-(methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene

: 762-42-5
dimethyl acetylenedicarboxylate

: 90330-50-0
dimethyl 4-acetyl-5-hydroxyphthalate

Guidance literature:: In benzene; for 24h; Ambient temperature;
DOI:10.1246/cl.1984.273

Reference yield: 53.0%

: 60804-09-3
4-acetyl-1-methyl-1-oxo-2H-1λ⁶-[1,2]thiazin-5-one

: 762-42-5
dimethyl acetylenedicarboxylate

: 90330-50-0
dimethyl 4-acetyl-5-hydroxyphthalate

Guidance literature:: In various solvent(s); for 6h; Heating;

Reference yield:

: 60804-09-3
4-acetyl-1-methyl-1-oxo-2H-1λ⁶-[1,2]thiazin-5-one

: 762-42-5
dimethyl acetylenedicarboxylate

: 94059-10-6
(E)-2-(4-Acetyl-5-hydroxy-1-methyl-1-oxo-1λ⁶-[1,2]thiazin-6-yl)-but-2-enedioic acid dimethyl ester

: 90330-50-0
dimethyl 4-acetyl-5-hydroxyphthalate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) DMSO, r.t., 30 min; 2.) reflux, 8 h;