Iridium(1+),carbonyl[3-chloro-6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine]bis(triphenylphosphine)-, perchlorate

Base Information

Chemical Name:Iridium(1+),carbonyl[3-chloro-6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine]bis(triphenylphosphine)-, perchlorate
CAS No.:90442-57-2
Molecular Formula:C₄₆H₃₉ClIrN₄OP₂*ClO₄
Molecular Weight:1052.91
Hs Code.:

Synonyms:Iridium(1+),carbonyl[3-chloro-6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine]bis(triphenylphosphine)-, perchlorate

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Chemical Property of Iridium(1+),carbonyl[3-chloro-6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine]bis(triphenylphosphine)-, perchlorate

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Technology Process of Iridium(1+),carbonyl[3-chloro-6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine]bis(triphenylphosphine)-, perchlorate

There total 1 articles about Iridium(1+),carbonyl[3-chloro-6-(3,5-dimethyl-1H-pyrazol-1-yl)pyridazine]bis(triphenylphosphine)-, perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: silver perchlorate

: 29334-67-6
3-chloro-6-(3,5-dimethylpyrazol-1-yl)pyridazine

: 90442-57-2
{Ir(carbon monoxide)(3-(3,5-dimethylpyrazol-1-yl)-6-chloro-pyridazine)(triphenylphosphine)2}ClO₄

Guidance literature:: In acetone; byproducts: AgCl; suspn. of Ir complex in acetone stirred, under N2, for 30 min with AgClO4, AgCl filtered off, filtrate added to acetone soln. of amine ligand, stirred for 15 min; concd. in vac., pptd. with ether, filtered off, washed with ether, air-dried, elem. anal.;
DOI:10.1016/S0277-5387(00)88052-3