Methanaminium,N-[3-(dimethylamino)-2-(phenylthio)-2-propenylidene]-N-methyl-,perchlorate

Base Information

Chemical Name:Methanaminium,N-[3-(dimethylamino)-2-(phenylthio)-2-propenylidene]-N-methyl-,perchlorate
CAS No.:90584-76-2
Molecular Formula:C13H19N2S.ClO4
Molecular Weight:334.824
Hs Code.:

Synonyms:Methanaminium,N-[3-(dimethylamino)-2-(phenylthio)-2-propenylidene]-N-methyl-,perchlorate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanaminium,N-[3-(dimethylamino)-2-(phenylthio)-2-propenylidene]-N-methyl-,perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanaminium,N-[3-(dimethylamino)-2-(phenylthio)-2-propenylidene]-N-methyl-,perchlorate

There total 4 articles about Methanaminium,N-[3-(dimethylamino)-2-(phenylthio)-2-propenylidene]-N-methyl-,perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(dimethylamino)-2-(phenylthio)-2-propenal

: NaClO_4.H₂ O

: 927-63-9,692-32-0
(E)-3-(dimethylamino)acrolein

: 882-33-7
diphenyldisulfane

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 90584-76-2
N-(3-(Dimethylamino)-2-(phenylthio)-2-propenylidene)-N-methylmethanaminium Perchlorate

Guidance literature:: With triethylamine; In dichloromethane; water; benzene;

Reference yield:

: 28074-23-9
phenylsulfenyl bromide

: 90584-76-2
N-(3-(Dimethylamino)-2-(phenylthio)-2-propenylidene)-N-methylmethanaminium Perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: 2) NaClO₄*H₂O / 1) benzene, 3 d, room temperature

With sodium perchlorate; triethylamine; In dichloromethane;
DOI:10.1021/jo00189a040

Reference yield:

: 882-33-7
diphenyldisulfane

: 90584-76-2
N-(3-(Dimethylamino)-2-(phenylthio)-2-propenylidene)-N-methylmethanaminium Perchlorate

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / CH₂Cl₂ / 0.17 h / 0 °C

2: Et₃N / CH₂Cl₂ / Ambient temperature

3: 2) NaClO₄*H₂O / 1) benzene, 3 d, room temperature

With sodium perchlorate; bromine; triethylamine; In dichloromethane;
DOI:10.1021/jo00189a040