Benzoic acid, 2-amino-5-hydroxy-, ethyl ester

Base Information

Chemical Name:Benzoic acid, 2-amino-5-hydroxy-, ethyl ester
CAS No.:90610-22-3
Molecular Formula:C9H11NO3
Molecular Weight:181.191
Hs Code.:

Synonyms:BENZOIC ACID,2-AMINO-5-HYDROXY-,ETHYL ESTER;ETHYL 5-HYDROXYANTHRANILATE;2-Amino-5-hydroxy-benzoesaeure-aethylester;2-AMINO-5-HYDROXYBENZOIC ACID ETHYL ESTER;

Suppliers and Price of Benzoic acid, 2-amino-5-hydroxy-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-AMINO-5-HYDROXYBENZOIC ACID ETHYL ESTER 95.00%
5MG
$ 503.70

Total 4 raw suppliers

Chemical Property of Benzoic acid, 2-amino-5-hydroxy-, ethyl ester

Chemical Property:

PSA：72.55000
LogP:1.73230

Purity/Quality:

99% ^*data from raw suppliers

2-AMINO-5-HYDROXYBENZOIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-amino-5-hydroxy-, ethyl ester

There total 3 articles about Benzoic acid, 2-amino-5-hydroxy-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 64-17-5
ethanol

: DL-N-(2-phenoxypropionyl)anthranilic acid

: 90610-22-3
ethyl 2-amino-5-hydroxybenzoate

Guidance literature:: With sulfuric acid; for 24h; Reflux;
DOI:10.1007/s12272-014-0353-1

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 90610-22-3
ethyl 2-amino-5-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 6 h / 20 °C

1.2: 12 h / 20 °C

2.1: sulfuric acid / 24 h / Reflux

With sulfuric acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1007/s12272-014-0353-1