Rhenium, triiodooxobis(triphenylarsine)-

Base Information

Chemical Name:Rhenium, triiodooxobis(triphenylarsine)-
CAS No.:90623-36-2
Molecular Formula:C36H30As2I3ORe
Molecular Weight:1195.4
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Rhenium, triiodooxobis(triphenylarsine)-

Chemical Property:

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Technology Process of Rhenium, triiodooxobis(triphenylarsine)-

There total 1 articles about Rhenium, triiodooxobis(triphenylarsine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10466-65-6
potassium perrhenate

: 603-32-7
triphenyl-arsane

: 90623-36-2
Re(O)I₃{As(C₆H₅)3}2

Guidance literature:: With HI; In water; prepared from KReO4, aq. HI and AsPh3 according to Johnson, N. P.; Lock, C. J. L.; Wilkinson, G. J. Chem. Soc. 1964, 1054-1066;
DOI:10.1021/ja00325a039

Reference yield: 40.0%

: 673-32-5
1-Phenylprop-1-yne

: 90623-36-2
Re(O)I₃{As(C₆H₅)3}2

: 90623-37-3
Re(O)I(C₆H₅CCCH₃)2

Guidance literature:: In benzene; of ReO(I)3(AsPh3)2 (as an unseparable mixt. with I2AsPh3) and PhCCMe inbenzene was stirred under inert atmosphere for 3 h; 1:4:0.15 mixt. of the three rotamers according to (1)H and (13)C NMR data; I2 in benzene was added dropwise, mixt. was filtered, filtrate evapd., residue was recrystd. from hexane, anal. pure complex was obtained by sublimation at 60°C (0.003 Torr); elem. anal.;
DOI:10.1021/ja00311a039

Reference yield:

: 90623-36-2
Re(O)I₃{As(C₆H₅)3}2

: 501-65-5
diphenyl acetylene

: 123170-29-6
Rhenium(O)I(PhCCPh)2

Guidance literature:: In not given; complex was formed in low yield but was difficult to sep. from the freeacetylene; mass spectral data;
DOI:10.1021/ja00311a039