PIPERIDINE-1-CARBOXAMIDINE HEMISULFATE

Base Information

• Chemical Name: PIPERIDINE-1-CARBOXAMIDINE HEMISULFATE
• CAS No.: 17238-53-8
• Molecular Formula: 2C₆H₁₃N₃*H₂O₄S
• Molecular Weight: 352.458

Synonyms:Piperidine-1-carboximidamide sulfate;1-Piperidinecarboxamidine,hemisulfate;piperidinylguanidinium sulfate;Piperidin-1-carbamidin,Sulfat;N-Carboxyamidinepiperidine sulfate;piperidine-1-carboxamidine,sulfate;piperidine-1-carboxamidine 1/2h2so;

Chemical Property of PIPERIDINE-1-CARBOXAMIDINE HEMISULFATE

Chemical Property:

• Boiling Point: 202.9°Cat760mmHg
• Flash Point: 76.5°C
• PSA: 189.20000
• Density: g/cm³
• LogP: 2.63540

Purity/Quality:

97% ^*data from raw suppliers

Bis(piperidine-1-carboximidamide) hemisulfate 97.0% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PIPERIDINE-1-CARBOXAMIDINE HEMISULFATE

There total 1 articles about PIPERIDINE-1-CARBOXAMIDINE HEMISULFATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

piperidine (110-89-4) + S-Methylisothiourea sulfate (867-44-7,147895-43-0) → piperidinylguanidinium sulfate (17238-53-8,94052-13-8,100417-03-6)

Guidance literature:

In ethanol; Yield given; Heating; 10-12 h;

DOI:10.1002/jhet.5570270708

Reference yield: 90.0%

2-(3-N,N-dimethylamino-prop-2-en-1-onyl)phenyldiphenylphosphine (877129-18-5) + piperidinylguanidinium sulfate (17238-53-8,94052-13-8,100417-03-6) → C6H4P(C6H5)2C4N2H2N(CH2)5 (1350639-43-8)

Guidance literature:

With potassium hydroxide; In ethanol; for 20h; Inert atmosphere; Reflux;

DOI:10.1002/ejic.201100659

Reference yield: 80.0%

piperidinylguanidinium sulfate (17238-53-8,94052-13-8,100417-03-6) + 2-bromobenzoic-acid (88-65-3) → 2-Piperidino-3,4-dihydro-chinazolon-(4) (33080-90-9)

Guidance literature:

piperidinylguanidinium sulfate; 2-bromobenzoic-acid; With caesium carbonate; In N,N-dimethyl-formamide; for 0.333333h; Inert atmosphere;

With copper(l) iodide; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 20h; Inert atmosphere;

DOI:10.1055/s-0029-1216871

upstream raw materials:

piperidine

S-Methylisothiourea sulfate

Downstream raw materials:

6-oxo-2-piperidin-1-yl-1,6-dihydro-pyrimidine-5-carboxylic acid ethyl ester

6-Benzyl-2-piperidin-1-yl-5,6,7,8-tetrahydro-3H-pyrido[4,3-d]pyrimidin-4-one

6-(4-Methyl-benzoyl)-2-piperidin-1-yl-5,6,7,8-tetrahydro-3H-pyrido[4,3-d]pyrimidin-4-one

6-(4-Chloro-benzoyl)-2-piperidin-1-yl-5,6,7,8-tetrahydro-3H-pyrido[4,3-d]pyrimidin-4-one

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