3-Methyl-3,7,11-triazaspiro[5.6]dodecane

Base Information

Chemical Name:3-Methyl-3,7,11-triazaspiro[5.6]dodecane
CAS No.:90703-74-5
Molecular Formula:C₁₀H₂₁N₃
Molecular Weight:183.297
Hs Code.:
DSSTox Substance ID:DTXSID20546571
Wikidata:Q82424443

Synonyms:3-Methyl-3,7,11-triazaspiro[5.6]dodecane;90703-74-5;DTXSID20546571

Suppliers and Price of 3-Methyl-3,7,11-triazaspiro[5.6]dodecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Methyl-3,7,11-triazaspiro[5.6]dodecane

Chemical Property:

XLogP3:-0.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:183.173547683
Heavy Atom Count:13
Complexity:162

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCC2(CC1)CNCCCN2

Technology Process of 3-Methyl-3,7,11-triazaspiro[5.6]dodecane

There total 3 articles about 3-Methyl-3,7,11-triazaspiro[5.6]dodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 111725-49-6
3-methyl-3,7,11-triazaspiro<5,6>dodec-11-ene

: 90703-74-5
3-methyl-3,7,11-triazaspiro<5,6>dodecane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 55 ℃; for 5h;
DOI:10.1007/BF00474359

Reference yield:

: 50675-21-3
N-methyl-piperidine-4-carboxaldehyde

: 90703-74-5
3-methyl-3,7,11-triazaspiro<5,6>dodecane

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Br₂ / acetic acid / 1.5 h / 20 °C

2: 34 percent / K₂CO₃ / acetonitrile; methanol; H₂O

3: 60 percent / LiAlH₄ / tetrahydrofuran / 5 h / 55 °C

With lithium aluminium tetrahydride; bromine; potassium carbonate; In tetrahydrofuran; methanol; water; acetic acid; acetonitrile;
DOI:10.1007/BF00474359

Reference yield:

: 111725-47-4
1-methyl-4-bromopiperidine-4-carboxaldehyde hydrobromide

: 90703-74-5
3-methyl-3,7,11-triazaspiro<5,6>dodecane

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / K₂CO₃ / acetonitrile; methanol; H₂O

2: 60 percent / LiAlH₄ / tetrahydrofuran / 5 h / 55 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1007/BF00474359