4-(Azidomethyl)-1,2-dimethoxybenzene

Base Information

• Chemical Name: 4-(Azidomethyl)-1,2-dimethoxybenzene
• CAS No.: 90807-80-0
• Molecular Formula: C9H11N3O2
• Molecular Weight: 193.205
• DSSTox Substance ID: DTXSID60655818
• Nikkaji Number: J1.514.346K
• Wikidata: Q82570115

Synonyms:4-(Azidomethyl)-1,2-dimethoxybenzene;90807-80-0;3,4-dimethoxybenzyl azide;SCHEMBL23070508;DTXSID60655818;EN300-1829505

Chemical Property of 4-(Azidomethyl)-1,2-dimethoxybenzene

Chemical Property:

• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 193.085126602
• Heavy Atom Count: 14
• Complexity: 216

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=C(C=C(C=C1)CN=[N+]=[N-])OC

Technology Process of 4-(Azidomethyl)-1,2-dimethoxybenzene

There total 6 articles about 4-(Azidomethyl)-1,2-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-bromomethyl-1,2-dimethoxybenzene (21852-32-4) → 4-(azidomethyl)-1,2-dimethoxybenzene (90807-80-0)

Guidance literature:

With sodium azide; In dimethyl sulfoxide; at 20 ℃; Inert atmosphere;

DOI:10.1021/acs.jmedchem.9b01269

Reference yield: 95.0%

(3,4-dimethoxyphenyl)methanol (93-03-8) → 4-(azidomethyl)-1,2-dimethoxybenzene (90807-80-0)

Guidance literature:

With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 - 20 ℃; for 15h; Inert atmosphere;

DOI:10.1002/ejoc.202101175

Reference yield: 94.0%

4-chloromethyl-1,2-dimethoxy-benzene (7306-46-9) → 4-(azidomethyl)-1,2-dimethoxybenzene (90807-80-0)

Guidance literature:

With sodium azide; In acetone; for 16h; Heating;

DOI:10.1016/S0040-4020(01)00402-1

upstream raw materials:

4-chloromethyl-1,2-dimethoxy-benzene

(3,4-dimethoxyphenyl)methanol

4-bromomethyl-1,2-dimethoxybenzene

vanillin

Downstream raw materials:

3,4-dimethoxy-benzaldehyde

veratronitrile

Veratric acid

4-((4-chlorophenyl)(hydroxyl)methyl)-1-(3,4-dimethoxybenzyl)-1H-1,2,3-triazole

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