4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-en-1-amine

Base Information

Chemical Name:4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-en-1-amine
CAS No.:90809-13-5
Molecular Formula:C₁₆H₂₅NO
Molecular Weight:247.381
Hs Code.:
DSSTox Substance ID:DTXSID00707289

Synonyms:90809-13-5;4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-en-1-amine;DTXSID00707289

Suppliers and Price of 4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-en-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-en-1-amine

Chemical Property:

PSA：12.47000
LogP:3.49130
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:8
Exact Mass:247.193614421
Heavy Atom Count:18
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CC=C(C)COCC1=CC=CC=C1

Technology Process of 4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-en-1-amine

There total 3 articles about 4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10575-25-4
4-diethylamino-2-butyn-1-ol

: 90809-13-5
(E)-4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-enylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / diethyl ether / Heating

2: NaH / 1.) THF, reflux, 1 h, 2.) room temperature

With sodium hydride; In diethyl ether;
DOI:10.1002/hlca.19900730516

Reference yield:

: 1838-94-4
isoprene epoxide

: 90809-13-5
(E)-4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-enylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / bis(dibenzylidenacetone)palladium, Ph₃P, 1,2-bis(diphenylphosphine)ethane, AcOH / 20 h / Ambient temperature

2: NaH / 1.) THF, reflux, 1 h, 2.) room temperature

With sodium hydride; acetic acid; triphenylphosphine; 1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium⁽⁰⁾;
DOI:10.1002/hlca.19900730516

Reference yield:

: 100-39-0
benzyl bromide

: 132364-34-2
(E)-4-(Diethylamino)-2-methylbut-2-en-1-ol

: 90809-13-5
(E)-4-(Benzyloxy)-N,N-diethyl-3-methylbut-2-enylamine

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, reflux, 1 h, 2.) room temperature;
DOI:10.1002/hlca.19900730516