4-Diethylaminobenzenesulphonyl chloride

Base Information

Chemical Name:4-Diethylaminobenzenesulphonyl chloride
CAS No.:90945-15-6
Molecular Formula:C10H14ClNO2S
Molecular Weight:247.746
Hs Code.:
DSSTox Substance ID:DTXSID601276608

Synonyms:90945-15-6;SCHEMBL3223255;USMOFKMCIDJIBZ-UHFFFAOYSA-N;DTXSID601276608;4-diethylaminobenzenesulphonyl chloride;AKOS006336256;4-(diethylamino)benzenesulfonyl chloride;4-(diethylamino)benzene-1-sulfonyl chloride;EN300-1987356

Suppliers and Price of 4-Diethylaminobenzenesulphonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Diethylaminobenzenesulphonyl chloride

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:247.0433776
Heavy Atom Count:15
Complexity:274

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)C1=CC=C(C=C1)S(=O)(=O)Cl

Technology Process of 4-Diethylaminobenzenesulphonyl chloride

There total 4 articles about 4-Diethylaminobenzenesulphonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 35478-73-0
N,N-diethylsulfanilic acid

: 90945-15-6
4-(diethylamino)-benzenesulphonyl chloride

Guidance literature:: With phosphorus pentachloride; In dichloromethane; for 4h; Heating;

Reference yield:

: 616-45-5
2-pyrrolidinon

: 109-72-8,29786-93-4
n-butyllithium

: diethylaminobenzenesulphonyl chloride

: 90945-15-6
4-(diethylamino)-benzenesulphonyl chloride

Guidance literature:: In tetrahydrofuran; hexane; di-isopropyl ether;

Reference yield:

: 91-66-7
N,N-diethylaniline

: 90945-15-6
4-(diethylamino)-benzenesulphonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl chlorosulfonate / CH₂Cl₂ / 2 h / Ambient temperature

2: 75 percent / 98 percent phosphorus pentachloride / CH₂Cl₂ / 4 h / Heating

With chlorosulfonate de trimethylsilyle; phosphorus pentachloride; In dichloromethane;