Bicyclo[3.2.1]octan-6-one, 7-(hydroxymethylene)-1-(4-methoxyphenyl)-5-methyl-

Base Information

Chemical Name:Bicyclo[3.2.1]octan-6-one, 7-(hydroxymethylene)-1-(4-methoxyphenyl)-5-methyl-
CAS No.:90995-60-1
Molecular Formula:C₁₇H₂₀O₃
Molecular Weight:272.344
Hs Code.:

Synonyms:

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Chemical Property of Bicyclo[3.2.1]octan-6-one, 7-(hydroxymethylene)-1-(4-methoxyphenyl)-5-methyl-

Chemical Property:

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Technology Process of Bicyclo[3.2.1]octan-6-one, 7-(hydroxymethylene)-1-(4-methoxyphenyl)-5-methyl-

There total 10 articles about Bicyclo[3.2.1]octan-6-one, 7-(hydroxymethylene)-1-(4-methoxyphenyl)-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1193-18-6
3-methylcyclohexen-2-one

: 90995-60-1
(1S,5R)-7-[1-Hydroxy-meth-(E)-ylidene]-1-(4-methoxy-phenyl)-5-methyl-bicyclo[3.2.1]octan-6-one

Guidance literature:: Multi-step reaction with 7 steps

1: 2.) KOH / 1.) 95percent EtOH, reflux, 3 h, 2.) H₂O, reflux, 36 h

2: conc. H₂SO₄, H₃BO₃ / Heating

3: 68 percent / AcOH, NH₄OAc / benzene / 20 h / Heating

4: 50 percent / CuI / diethyl ether

5: 1.) KOH, H₂O, 2.) 6M HCl

6: 1.) potassium t-butoxide, 2.) 5percent KOH / 1.) benzene, reflux, 2.) MeOH

7: NaH, MeOH / benzene

With hydrogenchloride; methanol; potassium hydroxide; copper(l) iodide; sulfuric acid; potassium tert-butylate; ammonium acetate; water; boric acid; sodium hydride; acetic acid; In diethyl ether; benzene;

Reference yield:

: 62733-86-2,192433-20-8
1-Methyl-3-oxo-cyclohexan-1-carbonsaeure

: 90995-60-1
(1S,5R)-7-[1-Hydroxy-meth-(E)-ylidene]-1-(4-methoxy-phenyl)-5-methyl-bicyclo[3.2.1]octan-6-one

Guidance literature:: Multi-step reaction with 6 steps

1: conc. H₂SO₄, H₃BO₃ / Heating

2: 68 percent / AcOH, NH₄OAc / benzene / 20 h / Heating

3: 50 percent / CuI / diethyl ether

4: 1.) KOH, H₂O, 2.) 6M HCl

5: 1.) potassium t-butoxide, 2.) 5percent KOH / 1.) benzene, reflux, 2.) MeOH

6: NaH, MeOH / benzene

With hydrogenchloride; methanol; potassium hydroxide; copper(l) iodide; sulfuric acid; potassium tert-butylate; ammonium acetate; water; boric acid; sodium hydride; acetic acid; In diethyl ether; benzene;

Reference yield:

: 56294-19-0
methyl 1-methyl-3-oxocyclohexane-1-carboxylate

: 90995-60-1
(1S,5R)-7-[1-Hydroxy-meth-(E)-ylidene]-1-(4-methoxy-phenyl)-5-methyl-bicyclo[3.2.1]octan-6-one

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / AcOH, NH₄OAc / benzene / 20 h / Heating

2: 50 percent / CuI / diethyl ether

3: 1.) KOH, H₂O, 2.) 6M HCl

4: 1.) potassium t-butoxide, 2.) 5percent KOH / 1.) benzene, reflux, 2.) MeOH

5: NaH, MeOH / benzene

With hydrogenchloride; methanol; potassium hydroxide; copper(l) iodide; potassium tert-butylate; ammonium acetate; water; sodium hydride; acetic acid; In diethyl ether; benzene;