3-chloro-N,N-dipropylbenzamide

Base Information

Chemical Name:3-chloro-N,N-dipropylbenzamide
CAS No.:5552-80-7
Molecular Formula:C13H18ClNO
Molecular Weight:239.7411
Hs Code.:
DSSTox Substance ID:DTXSID90349950
Wikidata:Q82125560

Synonyms:3-chloro-N,N-dipropylbenzamide;17271-10-2;3-Chloro-N,N-di-n-propylbenzaMide, 97per cent;CBMicro_049087;Cambridge id 5552807;SCHEMBL13911266;DTXSID90349950;Benzamide, 3-chloro-N,N-dipropyl-;AKOS003266023;BIM-0048969.P001;AB00088742-01;SR-01000212804;SR-01000212804-1

Suppliers and Price of 3-chloro-N,N-dipropylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-chloro-N,N-dipropylbenzamide

Chemical Property:

Vapor Pressure:2.16E-05mmHg at 25°C
Boiling Point:360.8°Cat760mmHg
Flash Point:172°C
Density:1.076g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:239.1076919
Heavy Atom Count:16
Complexity:214

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCN(CCC)C(=O)C1=CC(=CC=C1)Cl

Technology Process of 3-chloro-N,N-dipropylbenzamide

There total 3 articles about 3-chloro-N,N-dipropylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 583-61-9
2,3-Lutidine

: 105-58-8,76619-83-5
Diethyl carbonate

: 5552-80-7
ethyl 2-(3-methylpyridin-2-yl)acetate

Guidance literature:: 2,3-Lutidine; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

Diethyl carbonate; In tetrahydrofuran; hexane; at -60 - 20 ℃;

With hydrogenchloride; In tetrahydrofuran; hexane;

Reference yield:

: 583-61-9
2,3-Lutidine

: 541-41-3
chloroformic acid ethyl ester

: 5552-80-7
ethyl 2-(3-methylpyridin-2-yl)acetate

Guidance literature:: 2,3-Lutidine; With N,N,N,N,-tetramethylethylenediamine; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

chloroformic acid ethyl ester; In tetrahydrofuran; at -78 - 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2003.12.101