9H-Thioxanthene, 4-methyl-9-(2,3,5,6-tetramethylphenyl)-

Base Information

Chemical Name:9H-Thioxanthene, 4-methyl-9-(2,3,5,6-tetramethylphenyl)-
CAS No.:91127-80-9
Molecular Formula:C24H24S
Molecular Weight:344.521
Hs Code.:

Synonyms:

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Chemical Property of 9H-Thioxanthene, 4-methyl-9-(2,3,5,6-tetramethylphenyl)-

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Technology Process of 9H-Thioxanthene, 4-methyl-9-(2,3,5,6-tetramethylphenyl)-

There total 3 articles about 9H-Thioxanthene, 4-methyl-9-(2,3,5,6-tetramethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: 91127-80-9
4-methyl-9-(2,3,5,6-tetramethylphenyl)thioxanthene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium carbonate / hexamethylphosphoric acid triamide / 5 h / 100 °C

2: 90 percent / diethyl ether; tetrahydrofuran / 1 h / Heating

3: 90 percent / 80percent H₂SO₄ / H₂O / 0.67 h

With sulfuric acid; sodium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; water;

Reference yield:

: 94008-86-3
2-(2-methylphenylthio)benzaldehyde

: 91127-80-9
4-methyl-9-(2,3,5,6-tetramethylphenyl)thioxanthene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / diethyl ether; tetrahydrofuran / 1 h / Heating

2: 90 percent / 80percent H₂SO₄ / H₂O / 0.67 h

With sulfuric acid; In tetrahydrofuran; diethyl ether; water;

Reference yield:

: 137-06-4
2-thiocresol

: 91127-80-9
4-methyl-9-(2,3,5,6-tetramethylphenyl)thioxanthene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium carbonate / hexamethylphosphoric acid triamide / 5 h / 100 °C

2: 90 percent / diethyl ether; tetrahydrofuran / 1 h / Heating

3: 90 percent / 80percent H₂SO₄ / H₂O / 0.67 h

With sulfuric acid; sodium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; water;