2-(4-Chlorobutane-1-sulfonyl)-1-phenylethan-1-one

Base Information

Chemical Name:2-(4-Chlorobutane-1-sulfonyl)-1-phenylethan-1-one
CAS No.:91154-10-8
Molecular Formula:C12H15ClO3S
Molecular Weight:274.768
Hs Code.:
DSSTox Substance ID:DTXSID90532365
Wikidata:Q82404909

Synonyms:91154-10-8;2-(4-Chlorobutane-1-sulfonyl)-1-phenylethan-1-one;DTXSID90532365

Suppliers and Price of 2-(4-Chlorobutane-1-sulfonyl)-1-phenylethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Chlorobutane-1-sulfonyl)-1-phenylethan-1-one

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:274.0430432
Heavy Atom Count:17
Complexity:326

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)CS(=O)(=O)CCCCCl

Technology Process of 2-(4-Chlorobutane-1-sulfonyl)-1-phenylethan-1-one

There total 1 articles about 2-(4-Chlorobutane-1-sulfonyl)-1-phenylethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3708-04-1
2-methylsulfonyl-1-phenylethanone

: 109-70-6
1.3-chlorobromopropane

: 91154-10-8
2-(4-chlorobutyl)sulphonyl-1-phenylethanone

Guidance literature:: With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; Petroleum ether; 1.) THF, petroleum ether, 0 deg C, 30 min, 2.) hexane, 3.) THF, 0 deg C, 3h, 4.) up to rt;

Reference yield: 93.0%

: 91154-10-8
2-(4-chlorobutyl)sulphonyl-1-phenylethanone

: 91154-11-9
2-(4-iodobutyl)sulphonyl-1-phenylethanone

Guidance literature:: With sodium iodide; In acetone; for 3h; Heating;

Reference yield:

: 91154-10-8
2-(4-chlorobutyl)sulphonyl-1-phenylethanone

: 91154-12-0
2-benzoylthiane-1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaI / acetone / 3 h / Heating

2: 90 percent / aq. NaOH / ethylhexadecyldimethyl ammonium bromide / CH₂Cl₂ / 1 h

With sodium hydroxide; sodium iodide; hexadecyldimethylethylammonium bromide; In dichloromethane; acetone;