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109-70-6

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Amadis Chemical offer CAS#109-70-6;CAT#A802077
Cas No: 109-70-6
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
1-Bromo-3-chloropropane
Cas No: 109-70-6
No Data 1 Kilogram 30 Metric Ton/Day Zouping Sanhao Chemical Co., Ltd . Contact Supplier
1-Bromo-3-chloropropane
Cas No: 109-70-6
No Data No Data Metric Ton/Day Shandong Xinhua Pharmaceutical Co.,Ltd Contact Supplier
1-Bromo-3-chloropropane 109-70-6
Cas No: 109-70-6
No Data No Data No Data Hunan Russell Chemicals Technology Co.,Ltd Contact Supplier
1-Bromo-3-chloropropane
Cas No: 109-70-6
No Data No Data No Data Pure Chemistry Scientific Inc. Contact Supplier

109-70-6 Usage

Reactivity Profile

Halogenated aliphatic compounds, such as 1-Bromo-3-chloropropane, are moderately or very reactive. Reactivity generally decreases with increased degree of substitution of halogen for hydrogen atoms. Materials in this group are incompatible with strong oxidizing and reducing agents. Also, they are incompatible with many amines, nitrides, azo/diazo compounds, alkali metals, and epoxides.

General Description

A colorless liquid. Insoluble in water and denser than water. May be toxic by inhalation, ingestion or skin absorption. Used to make pharmaceuticals and other chemicals.

Fire Hazard

Some of these materials may burn, but none ignite readily. Containers may explode when heated.

Chemical Properties

clear liquid

Uses

1-Bromo-3-chloropropane can be used safer and equally efficient alternative to chloroform as a phase-separation agent in the 1-step method of RNA isolation from biological samples such as animal and p lant tissue.

Uses

A replacement for CHCl3 in RNA phase separations

Purification Methods

Wash it with conc H2SO4, water, 10% Na2CO3 solution, water again and then dry with CaCl2 and fractionally distil it just before use [Akagi et al. J Am Chem Soc 78 4034 1956]. [Beilstein 1 H 109, 1 IV 212.]

Air & Water Reactions

Insoluble in water.

Health Hazard

Inhalation of vapors or dust is extremely irritating. May cause burning of eyes and flow of tears. May cause coughing, difficult breathing and nausea. Brief exposure effects last only a few minutes. Exposure in an enclosed area may be very harmful. Fire will produce irritating, corrosive and/or toxic gases. Runoff from fire control or dilution water may cause pollution.
InChI:InChI=1/C3H6BrCl/c4-2-1-3-5/h1-3H2

109-70-6 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (B62404)  1-Bromo-3-chloropropane  99% 109-70-6 B62404-1KG 920.79CNY Detail
Aldrich (B62404)  1-Bromo-3-chloropropane  99% 109-70-6 B62404-250G 319.41CNY Detail
Alfa Aesar (A11395)  1-Bromo-3-chloropropane, 99%    109-70-6 5000g 2231.0CNY Detail
Alfa Aesar (A11395)  1-Bromo-3-chloropropane, 99%    109-70-6 1000g 555.0CNY Detail
Alfa Aesar (A11395)  1-Bromo-3-chloropropane, 99%    109-70-6 500g 309.0CNY Detail
Alfa Aesar (A11395)  1-Bromo-3-chloropropane, 99%    109-70-6 250g 180.0CNY Detail
Alfa Aesar (A11395)  1-Bromo-3-chloropropane, 99%    109-70-6 100g 108.0CNY Detail

109-70-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 1-Bromo-3-chloropropane

1.2 Other means of identification

Product number -
Other names Propane, 1-bromo-3-chloro-

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:109-70-6 SDS

109-70-6Synthetic route

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
With hydrogen bromide; dibenzoyl peroxide In benzene at 20℃; for 6h;92%
With hydrogen bromide
With hydrogen bromide
3-chloropropyl p-toluenesulfonate
632-02-0

3-chloropropyl p-toluenesulfonate

diethyl ether
60-29-7

diethyl ether

ethylmagnesium bromide

ethylmagnesium bromide

A

1-Chloropentane
543-59-9

1-Chloropentane

B

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

3-chloropropyl p-toluenesulfonate
632-02-0

3-chloropropyl p-toluenesulfonate

diethyl ether
60-29-7

diethyl ether

phenylmagnesium bromide

phenylmagnesium bromide

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

3-chloropropyl p-toluenesulfonate
632-02-0

3-chloropropyl p-toluenesulfonate

diethyl ether
60-29-7

diethyl ether

heptyl magnesium (1+); bromide

heptyl magnesium (1+); bromide

A

decyl chloride
1002-69-3

decyl chloride

B

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

propyl bromide
106-94-5

propyl bromide

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
With sulfuryl dichloride; dibenzoyl peroxide
With sulfuryl dichloride; dilauryl peroxide
With sulfuryl dichloride; dilauryl peroxide
With sulfuryl dichloride; dibenzoyl peroxide
With chlorine at 25 - 180℃;
1,3-Dichloropropane
142-28-9

1,3-Dichloropropane

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
With ethyl bromide; aluminum tri-bromide at 2 - 5℃;
1,3-Dichloropropane
142-28-9

1,3-Dichloropropane

A

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

B

1,3-dibromo-propane
109-64-8

1,3-dibromo-propane

Conditions
ConditionsYield
With ethyl bromide; aluminum tri-bromide at 2 - 5℃;
3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

2-bromo-1-chloropropane
3017-95-6, 127054-44-8, 130232-86-9

2-bromo-1-chloropropane

B

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
With hydrogen bromide
With hydrogen bromide
With hydrogen bromide
1-chloro-3-hydroxypropane
627-30-5

1-chloro-3-hydroxypropane

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
With sulfuric acid; hydrogen bromide dann Destillieren;
With phosphorus tribromide
With phosphorus tribromide
hydrogen bromide
10035-10-6, 12258-64-9

hydrogen bromide

bromine
7726-95-6

bromine

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
in Gegenwart von Feuchtigkeit;
hydrogen bromide
10035-10-6, 12258-64-9

hydrogen bromide

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

BiCl3

BiCl3

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
in Gegenwart von Feuchtigkeit;
hydrogen bromide
10035-10-6, 12258-64-9

hydrogen bromide

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

oxygen

oxygen

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
in Gegenwart von Feuchtigkeit;
p-toluenesulfonic acid-<γ-chloro-propyl>-ester

p-toluenesulfonic acid-<γ-chloro-propyl>-ester

alkyl magnesium bromide

alkyl magnesium bromide

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
With diethyl ether
sulfuryl dichloride
7791-25-5

sulfuryl dichloride

dilauryl peroxide
105-74-8

dilauryl peroxide

propyl bromide
106-94-5

propyl bromide

A

1-bromo-2-chloropropane
3017-96-7

1-bromo-2-chloropropane

B

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

sulfuryl dichloride
7791-25-5

sulfuryl dichloride

propyl bromide
106-94-5

propyl bromide

dibenzoyl peroxide
94-36-0

dibenzoyl peroxide

A

1-bromo-2-chloropropane
3017-96-7

1-bromo-2-chloropropane

B

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

hydrogen bromide
10035-10-6, 12258-64-9

hydrogen bromide

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

2-bromo-1-chloropropane
3017-95-6, 127054-44-8, 130232-86-9

2-bromo-1-chloropropane

B

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
at -18 - 18℃;
unter verschiedenen Bedingungen;
unter verschiedenen Bedingungen;
hydrogen bromide
10035-10-6, 12258-64-9

hydrogen bromide

acetic acid
64-19-7

acetic acid

3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

2-bromo-1-chloropropane
3017-95-6, 127054-44-8, 130232-86-9

2-bromo-1-chloropropane

B

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
at -18 - 18℃;
ethyl bromide
74-96-4

ethyl bromide

aluminium bromide
7727-15-3

aluminium bromide

1,3-Dichloropropane
142-28-9

1,3-Dichloropropane

A

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

B

1,3-dibromo-propane
109-64-8

1,3-dibromo-propane

Conditions
ConditionsYield
at 2 - 5℃;
3-chloroprop-1-ene
107-05-1

3-chloroprop-1-ene

A

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

B

CH2ClCHBrCH3

CH2ClCHBrCH3

Conditions
ConditionsYield
With hydrogen bromide at 100℃;
CH2BrCH2CH2Br

CH2BrCH2CH2Br

A

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

B

CH2ClCHBrCH3

CH2ClCHBrCH3

Conditions
ConditionsYield
With mercury dichloride
hydrogenchloride
7647-01-0

hydrogenchloride

1-bromo-3-propanol
627-18-9

1-bromo-3-propanol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Conditions
ConditionsYield
beim Kochen;
3-chloropropyl p-toluenesulfonate
632-02-0

3-chloropropyl p-toluenesulfonate

cyclohexyl magnesium (1+); bromide

cyclohexyl magnesium (1+); bromide

A

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

B

3-chloro-1-cyclohexyl-propane

3-chloro-1-cyclohexyl-propane

3-chloropropyl p-toluenesulfonate
632-02-0

3-chloropropyl p-toluenesulfonate

diethyl ether
60-29-7

diethyl ether

hexyl magnesium (1+); bromide

hexyl magnesium (1+); bromide

A

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

B

n-nonyl chloride

n-nonyl chloride

3-chloropropyl p-toluenesulfonate
632-02-0

3-chloropropyl p-toluenesulfonate

diethyl ether
60-29-7

diethyl ether

dodecyl magnesium (1+); bromide

dodecyl magnesium (1+); bromide

A

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

B

n-pentadecyl chloride

n-pentadecyl chloride

thiophenol
108-98-5

thiophenol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

3-chloropropyl phenyl sulfide
4911-65-3

3-chloropropyl phenyl sulfide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 25℃; for 12h;100%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 1h;98%
Stage #1: thiophenol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 1h; Inert atmosphere;
Stage #2: 1.3-chlorobromopropane In tetrahydrofuran at 0 - 20℃; for 24h; Inert atmosphere;
95%
Isobutyronitrile
78-82-0

Isobutyronitrile

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

5-chloro-2,2-dimethylpentanenitrile
4207-54-9

5-chloro-2,2-dimethylpentanenitrile

Conditions
ConditionsYield
With lithium hexamethyldisilazane at 70℃; for 16h;100%
With lithium hexamethyldisilazane at 70℃; for 16h;100%
With lithium hexamethyldisilazane at 70℃; for 16h;100%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

para-thiocresol
106-45-6

para-thiocresol

γ-chloropropyl 4-methylphenyl sulphide
3147-30-6

γ-chloropropyl 4-methylphenyl sulphide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃;100%
With sodium hydroxide In ethanol at 100℃;65%
With potassium hydroxide
2,3-dihydro-2H-furan
1191-99-7

2,3-dihydro-2H-furan

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

5-(3-chloropropyl)-2,3-dihydrofuran
110188-06-2

5-(3-chloropropyl)-2,3-dihydrofuran

Conditions
ConditionsYield
Stage #1: 2,3-dihydro-2H-furan With tert.-butyl lithium In tetrahydrofuran; pentane at -78 - 0℃; for 3h; Inert atmosphere;
Stage #2: 1.3-chlorobromopropane In tetrahydrofuran; pentane at -78℃; for 14h; Inert atmosphere;
100%
With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium 1.) THF, from -78 deg C to 0 deg C, 1.25 h, 2.) THF, from 0 deg C to 25 deg C, 7.33 h; Yield given. Multistep reaction;
2,6-dihydroxylacetophenone
699-83-2

2,6-dihydroxylacetophenone

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

2-(3-chlorophenoxy)-6-hydroxyacetophenone
105277-74-5

2-(3-chlorophenoxy)-6-hydroxyacetophenone

Conditions
ConditionsYield
With potassium carbonate In acetone for 24h; Heating;100%
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 4h;46%
With potassium carbonate In acetone
4-Phenylphenol
92-69-3

4-Phenylphenol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

4-(3-chloropropoxy)-1,1'-biphenyl
99472-05-6

4-(3-chloropropoxy)-1,1'-biphenyl

Conditions
ConditionsYield
With potassium carbonate In acetone for 24h; Williamson Ether Synthesis; Reflux;100%
With potassium carbonate In acetone for 24h; Heating;71%
With potassium carbonate In acetone for 24h; Heating;70%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

4-Hydroxyacetophenone
99-93-4

4-Hydroxyacetophenone

1-[4-(3-chloropropoxy)phenyl]ethanone
91427-23-5

1-[4-(3-chloropropoxy)phenyl]ethanone

Conditions
ConditionsYield
With potassium carbonate In acetone at 65℃; for 18h;100%
With potassium carbonate In acetone at 65℃;99%
With potassium carbonate In acetone at 65℃;99%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

meta-hydroxyacetanilide
621-42-1

meta-hydroxyacetanilide

N-<3-(3-chloropropoxy)phenyl>acetamide
78702-97-3

N-<3-(3-chloropropoxy)phenyl>acetamide

Conditions
ConditionsYield
With potassium carbonate In acetone for 16h; Heating;100%
With sodium hydroxide In ethanol for 8h; Heating;65%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

N-(3,3-dimethoxy-2-butylidene)isopropylamine
158220-74-7

N-(3,3-dimethoxy-2-butylidene)isopropylamine

N-(7-chloro-2,2-dimethoxy-3-heptylidene)isopropylamine
163679-86-5

N-(7-chloro-2,2-dimethoxy-3-heptylidene)isopropylamine

Conditions
ConditionsYield
With lithium diisopropyl amide In tetrahydrofuran; hexane 1.) 0 deg C, 3 h, 2.) rt, 20 h;100%
Stage #1: N-(3,3-dimethoxy-2-butylidene)isopropylamine With lithium diisopropyl amide In tetrahydrofuran; hexane at 0℃; for 3h;
Stage #2: 1.3-chlorobromopropane In tetrahydrofuran; hexane at 0 - 20℃; for 20h;
98%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

2-nitro-10H-indolo[3,2-b]quinoline
182123-57-5

2-nitro-10H-indolo[3,2-b]quinoline

2-nitro-10-chloropropylindolo[3,2-b]quinoline
214467-43-3

2-nitro-10-chloropropylindolo[3,2-b]quinoline

Conditions
ConditionsYield
With sodium hydroxide; dimethyl sulfoxide at 20℃; for 4h; Substitution;100%
benzoimidazole
51-17-2

benzoimidazole

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

1-(Benzimidazol-1-yl)-3-chloropropane
151029-72-0

1-(Benzimidazol-1-yl)-3-chloropropane

Conditions
ConditionsYield
Stage #1: benzoimidazole With sodium hydride In 1-methyl-pyrrolidin-2-one at 20℃; for 0.5h;
Stage #2: 1.3-chlorobromopropane In 1-methyl-pyrrolidin-2-one at 20 - 100℃; for 76h;
100%
With tetrabutylammomium bromide; sodium hydroxide In water at 60℃; for 2.08333h;62%
With sodium hydride 1) acetonitrile, reflux, 1 h; 2) acetonitrile, reflux, 2 h; Yield given; Multistep reaction;
With potassium carbonate In acetone for 12h; Reflux;
methyl 4'-hydroxy-4-biphenylcarboxylate
40501-41-5

methyl 4'-hydroxy-4-biphenylcarboxylate

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

Methyl 4'-(3-chloropropoxy)[1,1'-biphenyl]-4-carboxylate
372514-04-0

Methyl 4'-(3-chloropropoxy)[1,1'-biphenyl]-4-carboxylate

Conditions
ConditionsYield
With potassium carbonate In butanone for 24h; Heating;100%
With potassium carbonate In butanone92%
With potassium carbonate In butanone92%
2-fluoro-4-hydroxybenzonitrile
82380-18-5

2-fluoro-4-hydroxybenzonitrile

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

4-(3-chloropropoxy)-2-fluorobenzonitrile
873547-02-5

4-(3-chloropropoxy)-2-fluorobenzonitrile

Conditions
ConditionsYield
With potassium carbonate In butanone Heating;100%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

1-(3,5-difluoro-4-hydroxyphenyl)ethanone
133186-55-7

1-(3,5-difluoro-4-hydroxyphenyl)ethanone

1-[4-(3-chloro-propoxy)-3,5-difluoro-phenyl]-ethanone
1005402-88-9

1-[4-(3-chloro-propoxy)-3,5-difluoro-phenyl]-ethanone

Conditions
ConditionsYield
With potassium carbonate In acetone for 20h; Heating / reflux;100%
4-(5-methyl-4, 5,6,7-tetrahydro[1,3]oxazolo[4,5-c]pyridin-2-yl)phenol
1004764-46-8

4-(5-methyl-4, 5,6,7-tetrahydro[1,3]oxazolo[4,5-c]pyridin-2-yl)phenol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

2-[4-(3-chloropropoxy)phenyl]-5-methyl-4,5,6,7-tetrahydro[1,3]oxazolo[4,5-c]pyridine

2-[4-(3-chloropropoxy)phenyl]-5-methyl-4,5,6,7-tetrahydro[1,3]oxazolo[4,5-c]pyridine

Conditions
ConditionsYield
With potassium carbonate In butanone for 4h; Heating / reflux;100%
4-(4-acetyl-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-b]azepin-2-yl)phenol
1004764-62-8

4-(4-acetyl-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-b]azepin-2-yl)phenol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

4-acetyl-2-[4-(3-chloropropoxy)phenyl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-b]azepine

4-acetyl-2-[4-(3-chloropropoxy)phenyl]-5,6,7,8-tetrahydro-4H-[1,3]thiazolo[5,4-b]azepine

Conditions
ConditionsYield
With potassium carbonate In butanone for 20h; Heating / reflux;100%
In ethyl acetate for 20h; Reflux;100%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

5-hydroxy-1,3-dihydro-1-isoindolone
252061-66-8

5-hydroxy-1,3-dihydro-1-isoindolone

5-(3-chloro-propoxy)-2,3-dihydro-isoindol-1-one
928257-25-4

5-(3-chloro-propoxy)-2,3-dihydro-isoindol-1-one

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In acetonitrile for 18h; Heating / reflux;100%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

potassium thioacetate
10387-40-3

potassium thioacetate

thioacetic acid S-(3-chloropropyl) ester
13012-54-9

thioacetic acid S-(3-chloropropyl) ester

Conditions
ConditionsYield
In tetrahydrofuran for 1h; Heating;100%
4-Iodophenol
540-38-5

4-Iodophenol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

1-(3-chloropropoxy)-4-iodobenzene
273217-89-3

1-(3-chloropropoxy)-4-iodobenzene

Conditions
ConditionsYield
With potassium carbonate In acetone for 20h; Heating / reflux;100%
With potassium carbonate In acetone100%
With potassium carbonate In acetone Heating / reflux;98%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

7-hydroxy-6-methoxy-3-pivaloyloxymethyl-3,4-dihydroquinazolin-4-one
193002-25-4

7-hydroxy-6-methoxy-3-pivaloyloxymethyl-3,4-dihydroquinazolin-4-one

7-(3-chloropropoxy)-6-methoxy-3-((pivaloyloxy)methyl)-3,4-dihydroquinazolin-4-one
264208-49-3

7-(3-chloropropoxy)-6-methoxy-3-((pivaloyloxy)methyl)-3,4-dihydroquinazolin-4-one

Conditions
ConditionsYield
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃;100%
3-(3-Ethyl-1,2,4-oxadiazol-5-yl)-9H-β-carboline

3-(3-Ethyl-1,2,4-oxadiazol-5-yl)-9H-β-carboline

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

9-(3-Chloro-1-propyl)-3-(3-ethyl-1,2,4-oxadiazol-5-yl)-9H-β-carboline

9-(3-Chloro-1-propyl)-3-(3-ethyl-1,2,4-oxadiazol-5-yl)-9H-β-carboline

Conditions
ConditionsYield
In N,N-dimethyl-formamide; acetone; mineral oil100%
1,3-Bis(2-methyloropanoyloxy)-propane

1,3-Bis(2-methyloropanoyloxy)-propane

propane-1,3-diyl bis(2-methylpropanoate)

propane-1,3-diyl bis(2-methylpropanoate)

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

1,3-bis(2,2-dimethyl-5-chloropentanoyloxy)-propane
139483-62-8

1,3-bis(2,2-dimethyl-5-chloropentanoyloxy)-propane

Conditions
ConditionsYield
With lithium diisopropyl amide In tetrahydrofuran; water100%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

2-fluoro-4-hydroxybenzoic acid
65145-13-3

2-fluoro-4-hydroxybenzoic acid

3-chloropropyl 4-(3-chloropropoxy)-2-fluorobenzoate
911135-12-1

3-chloropropyl 4-(3-chloropropoxy)-2-fluorobenzoate

Conditions
ConditionsYield
With potassium carbonate In butanone at 80℃;100%
4-bromo-2-fluorophenol
2105-94-4

4-bromo-2-fluorophenol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

4-bromo-1-(3-chloro-propoxy)-2-fluoro-benzene
181807-91-0

4-bromo-1-(3-chloro-propoxy)-2-fluoro-benzene

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 3h; Product distribution / selectivity; Heating / reflux;100%
8-[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-yl)-ethyl]-1-phenyl-1,3,8-triaza-spiro[4.5]decan-4-one

8-[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-yl)-ethyl]-1-phenyl-1,3,8-triaza-spiro[4.5]decan-4-one

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

3-(3-chloro-propyl)-8-[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-yl)-ethyl]-1-phenyl-1,3,8-triaza-spiro[4.5]decan-4-one

3-(3-chloro-propyl)-8-[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-yl)-ethyl]-1-phenyl-1,3,8-triaza-spiro[4.5]decan-4-one

Conditions
ConditionsYield
Stage #1: 8-[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-yl)-ethyl]-1-phenyl-1,3,8-triaza-spiro[4.5]decan-4-one With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.5h;
Stage #2: 1.3-chlorobromopropane In tetrahydrofuran at 0 - 50℃; for 4h;
100%
tert-butyl 1H-indole-2-carboxylate
84117-86-2

tert-butyl 1H-indole-2-carboxylate

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

tert-butyl 1-(3-chloropropyl)-1H-indole-2-carboxylate
1352949-75-7

tert-butyl 1-(3-chloropropyl)-1H-indole-2-carboxylate

Conditions
ConditionsYield
Stage #1: tert-butyl 1H-indole-2-carboxylate With sodium hydride In N,N-dimethyl-formamide
Stage #2: 1.3-chlorobromopropane In N,N-dimethyl-formamide at 60℃; for 16h;
100%
1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

3,3-difluoro-1,3-dihydro-2H-indol-2-one
197067-27-9

3,3-difluoro-1,3-dihydro-2H-indol-2-one

1-(3-chloropropyl)-3,3-difluoroindolin-2-one
1352949-54-2

1-(3-chloropropyl)-3,3-difluoroindolin-2-one

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 16h;100%
3,5-difluoro-4-(hydroxymethyl)phenol

3,5-difluoro-4-(hydroxymethyl)phenol

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

[4-(3-chloropropoxy)-2,6-difluorophenyl]methanol

[4-(3-chloropropoxy)-2,6-difluorophenyl]methanol

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 3h; Reflux;100%
With potassium carbonate In acetonitrile for 3h; Reflux;96%
With potassium carbonate In acetonitrile for 3h; Reflux;96%
4-(4-hydroxy-phenyl)-piperidine-1-carboxylic acid tert-butyl ester
149377-19-5

4-(4-hydroxy-phenyl)-piperidine-1-carboxylic acid tert-butyl ester

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

tert-butyl 4-(4-(3-chloropropoxy)phenyl)piperidine-1-carboxylate

tert-butyl 4-(4-(3-chloropropoxy)phenyl)piperidine-1-carboxylate

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 80℃; for 16h;100%
With potassium carbonate In acetone at 90℃; for 40h;
1-tert-butyl 3-ethyl 4-oxopiperidine-1,3-dicarboxylate
98977-34-5

1-tert-butyl 3-ethyl 4-oxopiperidine-1,3-dicarboxylate

1,3-chlorobromopropane
109-70-6

1,3-chlorobromopropane

C16H26ClNO5

C16H26ClNO5

Conditions
ConditionsYield
Stage #1: 1-tert-butyl 3-ethyl 4-oxopiperidine-1,3-dicarboxylate With potassium tert-butylate In tetrahydrofuran at -20℃; for 0.5h;
Stage #2: 1.3-chlorobromopropane In tetrahydrofuran at 15℃; Inert atmosphere;
100%

109-70-6Related news

The molecular structures and conformational compositions of 1-Bromo-3-chloropropane (cas 109-70-6) and 1,3-diiodopropane, as determined by gas-phase electron diffraction and molecular mechanics calculations08/20/2019

The molecular structures and conformational compositions of 1-bromo-3-chloropropane (BCP) and 1,3-diiodopropane (DIP) have been studied by gas-phase electron diffraction at 27 and 38°C, respectively. BCP was found to exist as a mixture of the following four conformers, with estimated mole fract...detailed

C–Br bond fission mechanism of 1-Bromo-3-chloropropane (cas 109-70-6) at 234 and 265 nm08/19/2019

The photodissociation of 1-bromo-3-chloropropane was studied at 234 and 265 nm using ion velocity imaging technique. Bromine fragments in this study were produced via direct dissociation of C–Br bond. The speed and angular distributions of Br∗ and Br were measured. The appearance of chlorine fr...detailed

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