2-(Diphenylphosphoryl)quinoline

Base Information

Chemical Name:2-(Diphenylphosphoryl)quinoline
CAS No.:91239-45-1
Molecular Formula:C21H16NOP
Molecular Weight:329.338
Hs Code.:
DSSTox Substance ID:DTXSID80535446
Nikkaji Number:J3.074.556F
Wikidata:Q82409752

Synonyms:2-(Diphenylphosphoryl)quinoline;91239-45-1;SCHEMBL16401204;DTXSID80535446

Suppliers and Price of 2-(Diphenylphosphoryl)quinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 2-(Diphenylphosphoryl)quinoline

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:329.096951132
Heavy Atom Count:24
Complexity:431

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=O)(C2=CC=CC=C2)C3=NC4=CC=CC=C4C=C3

Technology Process of 2-(Diphenylphosphoryl)quinoline

There total 10 articles about 2-(Diphenylphosphoryl)quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2005-43-8
2-bromoquinoline

: 4559-70-0
Diphenylphosphine oxide

: 91239-45-1
diphenyl(quinolin-2-yl)phosphine oxide

Guidance literature:: With copper(l) iodide; 4-hydroxy-N-(2-methylnaphthalen-1-yl)picolinamide; sodium carbonate; In isopropyl alcohol; at 120 ℃; for 20h; Inert atmosphere; Schlenk technique;
DOI:10.1002/cjoc.202100354

Reference yield: 87.0%

: 612-62-4
2-Chloroquinoline

: 4559-70-0
Diphenylphosphine oxide

: 91239-45-1
diphenyl(quinolin-2-yl)phosphine oxide

Guidance literature:: With bis(triphenylphosphine)nickel(II) chloride; potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; Inert atmosphere;
DOI:10.1039/c2ob26874d

Reference yield: 84.0%

: 59-31-4
2-hydroxyquinoline

: 4559-70-0
Diphenylphosphine oxide

: 91239-45-1
diphenyl(quinolin-2-yl)phosphine oxide

Guidance literature:: 2-hydroxyquinoline; With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In acetonitrile; at 100 ℃; for 3h; Inert atmosphere;

Diphenylphosphine oxide; With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In acetonitrile; at 100 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2cc31718d