Hetisan

Base Information

• Chemical Name: Hetisan
• CAS No.: 39608-70-3
• Molecular Formula: C20H27N
• Molecular Weight: 281.43508
• Mol file: 39608-70-3.mol

Synonyms:

Chemical Property of Hetisan

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of Hetisan

There total 1 articles about Hetisan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C19H25NO (1032857-01-4) + Methyltriphenylphosphonium bromide (1779-49-3) → C20H27N (39608-70-3)

Guidance literature:

Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; for 0.0833333h;

C₁₉H₂₅NO; In hexane; toluene; at 70 ℃; for 19h;

DOI:10.1002/chem.200701290

Reference yield: 69.0%

C20H27N (39608-70-3) → epi-nominine + 15-dehydronominine (85352-52-9) + nominine (79808-87-0)

Guidance literature:

With tert.-butylhydroperoxide; selenium(IV) oxide; In dichloromethane; water; at 0 ℃; for 10h;

DOI:10.1002/chem.200701290

upstream raw materials:

C₁₉H₂₅NO

Methyltriphenylphosphonium bromide

Downstream raw materials:

15-dehydronominine

nominine

Refernces