Acetamide, N-[2-[(3R,4S)-4-amino-3-phenyl-1-piperidinyl]-2-oxoethyl]-,monomethanesulfonate

Base Information

Chemical Name:Acetamide, N-[2-[(3R,4S)-4-amino-3-phenyl-1-piperidinyl]-2-oxoethyl]-,monomethanesulfonate
CAS No.:913092-78-1
Molecular Formula:C15H21N3O2.CH4O3S
Molecular Weight:371.458
Hs Code.:

Synonyms:Acetamide, N-[2-[(3R,4S)-4-amino-3-phenyl-1-piperidinyl]-2-oxoethyl]-,monomethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetamide, N-[2-[(3R,4S)-4-amino-3-phenyl-1-piperidinyl]-2-oxoethyl]-,monomethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Acetamide, N-[2-[(3R,4S)-4-amino-3-phenyl-1-piperidinyl]-2-oxoethyl]-,monomethanesulfonate

There total 1 articles about Acetamide, N-[2-[(3R,4S)-4-amino-3-phenyl-1-piperidinyl]-2-oxoethyl]-,monomethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-75-2,98527-29-8
methanesulfonic acid

: 913092-77-0
N-{2-[(3R,4S)-4-amino-3-phenylpiperidin-1-yl]-2-oxoethyl}acetamide

: 913092-78-1
N-{2-[(3R,4S)-4-amino-3-phenylpiperidin-1-yl]-2-oxoethyl}acetamide methanesulfonate

Guidance literature:: In ethanol; at 25 - 65 ℃;

Reference yield: 90.0%

: 3'-formyl-4'-methoxybiphenyl-2-carbonitrile

: 913092-78-1
N-{2-[(3R,4S)-4-amino-3-phenylpiperidin-1-yl]-2-oxoethyl}acetamide methanesulfonate

: N-[2-((3R,4S)-4-{[(2'-cyano-4-methoxybiphenyl-3-yl)methyl]amino}-3-phenylpiperidin-1-yl)-2-oxoethyl]acetamide

Guidance literature:: 3'-formyl-4'-methoxybiphenyl-2-carbonitrile; N-{2-[(3R,4S)-4-amino-3-phenylpiperidin-1-yl]-2-oxoethyl}acetamide methanesulfonate; With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 10 - 35 ℃; for 12h;

With water; sodium hydrogencarbonate; In dichloromethane;

Reference yield: 75.0%

: 913092-72-5
2-(cyclopropylmethoxy)-5-[5-(trifluoromethyl)-1H-tetrazol-1-yl]benzaldehyde

: 913092-78-1
N-{2-[(3R,4S)-4-amino-3-phenylpiperidin-1-yl]-2-oxoethyl}acetamide methanesulfonate

: N-{2-[(3R,4S)-4-({2-(cyclopropylmethoxy)-5-[5-(trifluoromethyl)-1H-tetrazol-1-yl]benzyl}amino)-3-phenylpiperidin-1-yl]-2-oxoethyl}acetamide

Guidance literature:: 2-(cyclopropylmethoxy)-5-[5-(trifluoromethyl)-1H-tetrazol-1-yl]benzaldehyde; N-{2-[(3R,4S)-4-amino-3-phenylpiperidin-1-yl]-2-oxoethyl}acetamide methanesulfonate; With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 10 - 35 ℃; for 1h;

With water; In dichloromethane;

With sodium hydrogencarbonate; In dichloromethane; water; ethyl acetate;