Technology Process of 1,3-Propanediol, 1-(2-fluorophenyl)-, 1-acetate
There total 4 articles about 1,3-Propanediol, 1-(2-fluorophenyl)-, 1-acetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 61 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating
2: 57 percent / sodium hydroxide / trioctyl(methyl)ammonium chloride / CH2Cl2; H2O / 360 h / Heating
3: 86 percent / benzene / 5 h / Heating
4: 93 percent / dihydrogen / 10percent palladium on charcoal / ethanol
With
sodium hydroxide; lithium aluminium tetrahydride; hydrogen;
palladium on activated charcoal; Aliquat 336;
In
diethyl ether; ethanol; dichloromethane; water; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 57 percent / sodium hydroxide / trioctyl(methyl)ammonium chloride / CH2Cl2; H2O / 360 h / Heating
2: 86 percent / benzene / 5 h / Heating
3: 93 percent / dihydrogen / 10percent palladium on charcoal / ethanol
With
sodium hydroxide; hydrogen;
palladium on activated charcoal; Aliquat 336;
In
ethanol; dichloromethane; water; benzene;