Ethyl 2,3,4,9-tetrahydro-1H-pyrido(3,4-b)indole-1-acetate

Base Information

Chemical Name:Ethyl 2,3,4,9-tetrahydro-1H-pyrido(3,4-b)indole-1-acetate
CAS No.:94135-47-4
Molecular Formula:C15H18 N2 O2
Molecular Weight:258.32
Hs Code.:2933990090
European Community (EC) Number:302-916-9
DSSTox Substance ID:DTXSID90916328
Nikkaji Number:J368.304D
Mol file:94135-47-4.mol

Synonyms:94135-47-4;EINECS 302-916-9;Ethyl 2,3,4,9-tetrahydro-1H-pyrido(3,4-b)indole-1-acetate;ethyl 2-(2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetate;ETHYL 2,3,4,9-TETRAHYDRO-1H-PYRIDO[3,4-B]INDOLE-1-ACETATE;SCHEMBL8321835;DTXSID90916328;Ethyl (2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)acetate;1H-Pyrido[3,4-b]indole-1-aceticacid,2,3,4,9-tetrahydro-,ethyl ester;2,3,4,9-Tetrahydro-1H-pyrido[3,4-b]indole-1-acetic acid ethyl ester

Suppliers and Price of Ethyl 2,3,4,9-tetrahydro-1H-pyrido(3,4-b)indole-1-acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Ethyl 2,3,4,9-tetrahydro-1H-pyrido(3,4-b)indole-1-acetate

Chemical Property:

Vapor Pressure:1.15E-07mmHg at 25°C
Boiling Point:431.9°C at 760 mmHg
Flash Point:215°C
PSA：54.12000
Density:1.18g/cm³
LogP:2.63670
XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:258.136827821
Heavy Atom Count:19
Complexity:334

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC1C2=C(CCN1)C3=CC=CC=C3N2

Technology Process of Ethyl 2,3,4,9-tetrahydro-1H-pyrido(3,4-b)indole-1-acetate

There total 4 articles about Ethyl 2,3,4,9-tetrahydro-1H-pyrido(3,4-b)indole-1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 61-54-1
tryptamine

: 262293-82-3
3,3-dimethoxypropionic acid ethyl ester

: 94135-47-4
1-ethoxycarbonylmethyl-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2017.08.026

Reference yield: 46.0%

: 343-94-2
tryptamine hydochloride

: 2401-96-9
carboethoxypyruvic acid

: 94135-47-4
1-ethoxycarbonylmethyl-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: In ethanol; for 48h; Reflux;
DOI:10.1002/ddr.21494

Reference yield:

: 1038998-74-1
C₂₂H₂₄N₂O₂

: 94135-47-4
1-ethoxycarbonylmethyl-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: C₂₂H₂₄N₂O₂; With hydrogenchloride; In ethanol;

With 10% Pd/C; hydrogen; In ethanol; at 20 ℃; for 12h; under 760.051 Torr;

With triethylamine;
DOI:10.1002/anie.200800566