Benzamide, 2-(diphenylphosphino)-N-phenyl-

Base Information

Chemical Name:Benzamide, 2-(diphenylphosphino)-N-phenyl-
CAS No.:91410-02-5
Molecular Formula:C25H20NOP
Molecular Weight:381.414
Hs Code.:
DSSTox Substance ID:DTXSID90477368
Nikkaji Number:J1.988.510K
Wikidata:Q82309841

Synonyms:91410-02-5;2-(Diphenylphosphino)-N-phenylbenzamide;Benzamide, 2-(diphenylphosphino)-N-phenyl-;SCHEMBL21568081;DTXSID90477368

Suppliers and Price of Benzamide, 2-(diphenylphosphino)-N-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzamide, 2-(diphenylphosphino)-N-phenyl-

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:381.128251259
Heavy Atom Count:28
Complexity:459

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=O)C2=CC=CC=C2P(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Benzamide, 2-(diphenylphosphino)-N-phenyl-

There total 1 articles about Benzamide, 2-(diphenylphosphino)-N-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-90-7
chlorobenzene

: 343254-74-0
triphenylphosphine-2-carboxamide

: 91410-02-5
o-(diphenylphosphino)-N-phenylbenzamide

Guidance literature:: With pyridine; In tetrahydrofuran;
DOI:10.1021/ja00329a069

Reference yield: 95.0%

: [Pd(phenylazophenyl(-1H))(μ-OH)]2

: 91410-02-5
o-(diphenylphosphino)-N-phenylbenzamide

: 690199-17-8
[Pd(phenylazophenyl(-1H))(2-diphenylphosphine-N-phenylbenzamide(-1H))]

Guidance literature:: In dichloromethane; to soln. of Pd complex in CH2Cl2 added solid 2-diphenylphosphinebenzamide (molar ratio 1:2); soln. stirred for 30 min; filtered through Celite; concd. to half vol. (vac.); hexane added; ppt. filtered off; dried (air); recrystd. (CH2Cl2-hexane); elem. anal.;
DOI:10.1039/b310843k

Reference yield: 93.0%

: potassium tetrachloroplatinate

: 91410-02-5
o-(diphenylphosphino)-N-phenylbenzamide

: 98838-49-4
trans-dichlorobis(o-(diphenylphosphino)-N-phenylbenzamide)platinum(II)

Guidance literature:: In water; acetonitrile; dissolving Pt complex in aq. CH3CN under N2 atmosphere; equilibrating on oil bath at 60°C; dropwise addn. of 2 equiv. of ligand in CH3CNover 5 min; stirring for 1 h; pptn.; cooling to room temp.;; filtration; 3 fold washing with water, ethanol and then with pentane; drying in vac.; elem. anal.;;