1,2-Propanedione, 1-(3,4,5-trimethoxyphenyl)-

Base Information

Chemical Name:1,2-Propanedione, 1-(3,4,5-trimethoxyphenyl)-
CAS No.:91497-93-7
Molecular Formula:C12H14O5
Molecular Weight:238.24
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Propanedione, 1-(3,4,5-trimethoxyphenyl)-

Chemical Property:

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Technology Process of 1,2-Propanedione, 1-(3,4,5-trimethoxyphenyl)-

There total 5 articles about 1,2-Propanedione, 1-(3,4,5-trimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 657393-37-8
(1S,2S)-1-(3,4,5-trimethoxyphenyl)propane-1,2-diol

: 91497-93-7
1-<3,4,5-Trimethoxy-phenyl>-propandion-(1,2)

: 657393-38-9
(2S)-hydroxy-1-(3,4,5-trimethoxy-phenyl)-propan-1-one

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; at 20 ℃; for 5h; ultrasound;
DOI:10.1016/j.tetlet.2004.12.073

Reference yield: 64.0%

: 1449657-86-6
C₁₂H₁₄O₃

: 91497-93-7
1-<3,4,5-Trimethoxy-phenyl>-propandion-(1,2)

Guidance literature:: With ruthenium trichloride; [bis(acetoxy)iodo]benzene; water; In dichloromethane; at 20 ℃; for 2h; Cooling with ice;
DOI:10.1021/acs.jmedchem.1c00413

Reference yield:

: 24313-88-0
3,4,5-Trimethoxyaniline

: 91497-93-7
1-<3,4,5-Trimethoxy-phenyl>-propandion-(1,2)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; hydrogenchloride / tetrahydrofuran; water / 0.33 h / 0 °C

1.2: 1.33 h / 20 °C / Cooling with ice

2.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / N,N-dimethyl-formamide / 16 h / 90 °C / Inert atmosphere

3.1: [bis(acetoxy)iodo]benzene; ruthenium trichloride; water / dichloromethane / 2 h / 20 °C / Cooling with ice

With hydrogenchloride; ruthenium trichloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; [bis(acetoxy)iodo]benzene; water; triethylamine; sodium nitrite; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 1.1: |Sandmeyer Reaction / 1.2: |Sandmeyer Reaction / 2.1: |Sonogashira Cross-Coupling;
DOI:10.1021/acs.jmedchem.1c00413