1,1'-(2-Methylprop-1-ene-1,1-diyl)bis(4-bromobenzene)

Base Information

Chemical Name:1,1'-(2-Methylprop-1-ene-1,1-diyl)bis(4-bromobenzene)
CAS No.:26957-40-4
Molecular Formula:C16H14 Br2
Molecular Weight:366.095
Hs Code.:
NSC Number:143625
DSSTox Substance ID:DTXSID00301468
Wikidata:Q82045423

Synonyms:26957-40-4;1,1'-(2-methylprop-1-ene-1,1-diyl)bis(4-bromobenzene);NSC143625;DTXSID00301468;NSC-143625

Suppliers and Price of 1,1'-(2-Methylprop-1-ene-1,1-diyl)bis(4-bromobenzene)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,1'-(2-Methylprop-1-ene-1,1-diyl)bis(4-bromobenzene)

Chemical Property:

Boiling Point:394.7°Cat760mmHg
Flash Point:225.2°C
Density:1.49g/cm³
XLogP3:6.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:365.94418
Heavy Atom Count:18
Complexity:264

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C(C1=CC=C(C=C1)Br)C2=CC=C(C=C2)Br)C

Technology Process of 1,1'-(2-Methylprop-1-ene-1,1-diyl)bis(4-bromobenzene)

There total 3 articles about 1,1'-(2-Methylprop-1-ene-1,1-diyl)bis(4-bromobenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.9%

: 101167-45-7
1,1-bis(4-bromophenyl)-2-methylpropanol

: 26957-40-4
1,1-bis(4-bromophenyl)-2-methylpropene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 1h; Heating;

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 26957-40-4
1,1-bis(4-bromophenyl)-2-methylpropene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, 10 min, 2.) THF, hexane, 2 h

2: 93.9 percent / p-toluenesulfonic acid / benzene / 1 h / Heating

With n-butyllithium; toluene-4-sulfonic acid; In benzene;

Reference yield:

: 3988-03-2
bis(4-bromophenyl)methanone

: 920-39-8
isopropylmagnesium bromide

: 26957-40-4
1,1-bis(4-bromophenyl)-2-methylpropene

Guidance literature:: With diethyl ether; Dehydratisierung des gebildeten Alkohols durch Erhitzen unter vermindertem Druck;
DOI:10.1039/jr9480000261