Technology Process of Benzeneacetic acid, a-hydroxy-a-phenyl-,
1-[(2,2-dipropyl-1,3-dioxolan-4-yl)methyl]-4-piperidinyl ester
There total 4 articles about Benzeneacetic acid, a-hydroxy-a-phenyl-,
1-[(2,2-dipropyl-1,3-dioxolan-4-yl)methyl]-4-piperidinyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95.5 percent / K2CO3 / acetonitrile / 16 h / Heating
2: 1.) sodium hydride / 1.) oil, 80 deg C
With
sodium hydride; potassium carbonate;
In
acetonitrile;
DOI:10.1248/cpb.32.967
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85.7 percent / stannic chloride / CCl4 / 2.5 h / Ambient temperature
2: 95.5 percent / K2CO3 / acetonitrile / 16 h / Heating
3: 1.) sodium hydride / 1.) oil, 80 deg C
With
tin(IV) chloride; sodium hydride; potassium carbonate;
In
tetrachloromethane; acetonitrile;
DOI:10.1248/cpb.32.967
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95.5 percent / K2CO3 / acetonitrile / 16 h / Heating
2: 1.) sodium hydride / 1.) oil, 80 deg C
With
sodium hydride; potassium carbonate;
In
acetonitrile;
DOI:10.1248/cpb.32.967
