5H-Pyrrolo[3,4-b]pyridine-3-carboxylic acid, 4-(2,4-dichlorophenyl)-6-[1-[(1,1-dimethylethoxy)carbonyl]-4-piperidinyl]- 6,7-dihydro-2-methyl-5-oxo-

Base Information

• Chemical Name: 5H-Pyrrolo[3,4-b]pyridine-3-carboxylic acid, 4-(2,4-dichlorophenyl)-6-[1-[(1,1-dimethylethoxy)carbonyl]-4-piperidinyl]- 6,7-dihydro-2-methyl-5-oxo-
• CAS No.: 915297-19-7
• Molecular Formula: C25H27Cl2N3O5
• Molecular Weight: 520.412

Synonyms:

Chemical Property of 5H-Pyrrolo[3,4-b]pyridine-3-carboxylic acid, 4-(2,4-dichlorophenyl)-6-[1-[(1,1-dimethylethoxy)carbonyl]-4-piperidinyl]- 6,7-dihydro-2-methyl-5-oxo-

Chemical Property:

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Useful:

Technology Process of 5H-Pyrrolo[3,4-b]pyridine-3-carboxylic acid, 4-(2,4-dichlorophenyl)-6-[1-[(1,1-dimethylethoxy)carbonyl]-4-piperidinyl]- 6,7-dihydro-2-methyl-5-oxo-

There total 2 articles about 5H-Pyrrolo[3,4-b]pyridine-3-carboxylic acid, 4-(2,4-dichlorophenyl)-6-[1-[(1,1-dimethylethoxy)carbonyl]-4-piperidinyl]- 6,7-dihydro-2-methyl-5-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzyl 6-(1-(tert-butoxycarbonyl)piperidin-4-yl)-4-(2,4-dichlorophenyl)-2-methyl-5-oxo-6,7-dihydro-5H-pyrrolo[3,4-b]pyridine-3-carboxylate (915297-18-6) → 6-(1-(tert-butoxycarbonyl)piperidin-4-yl)-4-(2,4-dichlorophenyl)-2-methyl-5-oxo-6,7-dihydro-5H-pyrrolo[3,4-b]pyridine-3-carboxylic acid (915297-19-7)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 2h;

Reference yield:

→ 6-(1-(tert-butoxycarbonyl)piperidin-4-yl)-4-(2,4-dichlorophenyl)-2-methyl-5-oxo-6,7-dihydro-5H-pyrrolo[3,4-b]pyridine-3-carboxylic acid (915297-19-7)

Guidance literature:

Reference yield:

6-(1-(tert-butoxycarbonyl)piperidin-4-yl)-4-(2,4-dichlorophenyl)-2-methyl-5-oxo-6,7-dihydro-5H-pyrrolo[3,4-b]pyridine-3-carboxylic acid (915297-19-7) → C25H26Cl3N3O4

Guidance literature:

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;

upstream raw materials:

Benzyl 6-(1-(tert-butoxycarbonyl)piperidin-4-yl)-4-(2,4-dichlorophenyl)-2-methyl-5-oxo-6,7-dihydro-5H-pyrrolo[3,4-b]pyridine-3-carboxylate

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