Technology Process of Stannane, (1,2-diphenyl-1-propenyl)trimethyl-, (E)-
There total 2 articles about Stannane, (1,2-diphenyl-1-propenyl)trimethyl-, (E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
benzene-d6;
Irradiation (UV/VIS); Sn-complex in C6D6 was irradiated; monitored by NMR;
DOI:10.1039/DT9840000909
- Guidance literature:
-
In
diethyl ether; hexane; benzene;
n-BuLi in hexane was added to ligand in ether-benzene at -55°C, Sn-complex in ether-benzene was added to mixt. (5 min), after stirring for 2 min soln. was poured into NH4Cl; organic layer was sepd., washed with H2O, dried over Na2SO4, ether was removed under vac., crude ppt. was dissolved in ether and MeOH, cooled to -80°C; elem. anal.;
DOI:10.1039/DT9840000909
- Guidance literature:
-
In
benzene-d6;
Irradiation (UV/VIS); Sn-complex in C6D6 was irradiated; monitored by NMR;
DOI:10.1039/DT9840000909
