1H-Pyrazole-1-carboxylic acid, 3-[[3-[(3,4-dihydro-2-methyl-1,1-dioxido-2H-5,1,2-benzoxathiazepin-7-yl )oxy]-5-[(1S)-2-methoxy-1-methylethoxy]benzoyl]amino]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:1H-Pyrazole-1-carboxylic acid, 3-[[3-[(3,4-dihydro-2-methyl-1,1-dioxido-2H-5,1,2-benzoxathiazepin-7-yl )oxy]-5-[(1S)-2-methoxy-1-methylethoxy]benzoyl]amino]-, 1,1-dimethylethyl ester
CAS No.:915771-54-9
Molecular Formula:C28H34N4O9S
Molecular Weight:602.665
Hs Code.:

1H-Pyrazole-1-carboxylic acid,
3-[[3-[(3,4-dihydro-2-methyl-1,1-dioxido-2H-5,1,2-benzoxathiazepin-7-yl
)oxy]-5-[(1S)-2-methoxy-1-methylethoxy]benzoyl]amino]-,
1,1-dimethylethyl ester

Synonyms:

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Chemical Property of 1H-Pyrazole-1-carboxylic acid, 3-[[3-[(3,4-dihydro-2-methyl-1,1-dioxido-2H-5,1,2-benzoxathiazepin-7-yl )oxy]-5-[(1S)-2-methoxy-1-methylethoxy]benzoyl]amino]-, 1,1-dimethylethyl ester

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Technology Process of 1H-Pyrazole-1-carboxylic acid, 3-[[3-[(3,4-dihydro-2-methyl-1,1-dioxido-2H-5,1,2-benzoxathiazepin-7-yl )oxy]-5-[(1S)-2-methoxy-1-methylethoxy]benzoyl]amino]-, 1,1-dimethylethyl ester

There total 2 articles about 1H-Pyrazole-1-carboxylic acid, 3-[[3-[(3,4-dihydro-2-methyl-1,1-dioxido-2H-5,1,2-benzoxathiazepin-7-yl )oxy]-5-[(1S)-2-methoxy-1-methylethoxy]benzoyl]amino]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 863504-84-1
3-aminopyrazole-1-carboxylic acid tert-butyl ester

: 915771-54-9
1,1-dimethylethyl 3-{[(3-[(2-methyl-1,1-dioxido-3,4-dihydro-2H-5,1,2-benzoxathiazepin-7-yl)oxy]-5-{[(1S)-1-methyl-2-(methyloxy)ethyl]oxy}phenyl)carbonyl]amino}-1H-pyrazole-1-carboxylate

Guidance literature:: 3-[(2-methyl-1,1-dioxido-3,4-dihydro-2H-5,1,2-benzoxathiazepin-7-yl)oxy]-5-{[(1S)-1-methyl-2-(methyloxy)ethyl]oxy}benzoic acid; With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In dichloromethane; for 1h;

3-aminopyrazole-1-carboxylic acid tert-butyl ester; With pyridine; In dichloromethane;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 915771-54-9
1,1-dimethylethyl 3-{[(3-[(2-methyl-1,1-dioxido-3,4-dihydro-2H-5,1,2-benzoxathiazepin-7-yl)oxy]-5-{[(1S)-1-methyl-2-(methyloxy)ethyl]oxy}phenyl)carbonyl]amino}-1H-pyrazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 2.08 h / 20 °C

2.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 1 h

With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;