Phenylbis(2,4,6-trimethoxyphenyl)phosphine

Base Information

• Chemical Name: Phenylbis(2,4,6-trimethoxyphenyl)phosphine
• CAS No.: 91608-16-1
• Molecular Formula: C₂₄H₂₇O₆P
• Molecular Weight: 442.449
• DSSTox Substance ID: DTXSID501266028

Synonyms:SCHEMBL10702455;DTXSID501266028;Phenylbis(2,4,6-trimethoxyphenyl)phosphine;91608-16-1

Chemical Property of Phenylbis(2,4,6-trimethoxyphenyl)phosphine

Chemical Property:

• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 9
• Exact Mass: 442.15452557
• Heavy Atom Count: 31
• Complexity: 452

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC(=C(C(=C1)OC)P(C2=CC=CC=C2)C3=C(C=C(C=C3OC)OC)OC)OC

Technology Process of Phenylbis(2,4,6-trimethoxyphenyl)phosphine

There total 1 articles about Phenylbis(2,4,6-trimethoxyphenyl)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

1,2,3-trimethoxybenzene (621-23-8) + Dichlorophenylphosphine (644-97-3) → bis(2,4,6-trimethoxyphenyl)phenylphosphine (91608-16-1)

Guidance literature:

With zinc(II) chloride; at 65 ℃; Inert atmosphere;

DOI:10.1021/acs.joc.6b00872

Reference yield: 97.0%

bis(2,4,6-trimethoxyphenyl)phenylphosphine (91608-16-1) + methyl iodide (74-88-4) → C25H29O6P*HI

Guidance literature:

at 50 ℃; for 0.25h; Inert atmosphere;

DOI:10.1021/acs.joc.6b00872

Reference yield:

bis(2,4,6-trimethoxyphenyl)phenylphosphine (91608-16-1) → Phenyl-(2,4,6-trimethoxy-phenyl)-phosphane

Guidance literature:

With ammonia; sodium; at -78 ℃; for 4h;

upstream raw materials:

1,2,3-trimethoxybenzene

Dichlorophenylphosphine

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