Perchloric acid;tris(2,4,6-trimethoxyphenyl)phosphane

Base Information

Chemical Name:Perchloric acid;tris(2,4,6-trimethoxyphenyl)phosphane
CAS No.:91608-17-2
Molecular Formula:C27H33O9P.ClHO4
Molecular Weight:632.986
Hs Code.:
DSSTox Substance ID:DTXSID40530452

Synonyms:91608-17-2;DTXSID40530452;Perchloric acid--tris(2,4,6-trimethoxyphenyl)phosphane (1/1)

Suppliers and Price of Perchloric acid;tris(2,4,6-trimethoxyphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Perchloric acid;tris(2,4,6-trimethoxyphenyl)phosphane

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:13
Rotatable Bond Count:12
Exact Mass:632.1425558
Heavy Atom Count:42
Complexity:644

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)OC)P(C2=C(C=C(C=C2OC)OC)OC)C3=C(C=C(C=C3OC)OC)OC)OC.OCl(=O)(=O)=O

Technology Process of Perchloric acid;tris(2,4,6-trimethoxyphenyl)phosphane

There total 2 articles about Perchloric acid;tris(2,4,6-trimethoxyphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 91608-15-0
tris(2,4,6-trimethoxyphenyl)phosphine

: 91608-17-2
tris(2,4,6-trimethoxyphenyl)phosphonium perchlorate

Guidance literature:: With ammonium perchlorate; In ethanol;
DOI:10.1039/c39840000482

Reference yield:

: 34425-71-3
1-lithium-2,4,6-trimethoxybenzene

: 91608-17-2
tris(2,4,6-trimethoxyphenyl)phosphonium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / P(OPh)3 / diethyl ether / 0 deg C to r.t.

2: 88 percent / NH₄ClO₄ / ethanol

With triphenyl phosphite; ammonium perchlorate; In diethyl ether; ethanol;
DOI:10.1039/c39840000482