Carbamic acid, N-[2-[[[2,6-bis[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-4-[(2-propyn- 1-ylamino)carbonyl]phenoxy]carbonyl]methylamino]ethyl]-N-methyl-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, N-[2-[[[2,6-bis[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-4-[(2-propyn- 1-ylamino)carbonyl]phenoxy]carbonyl]methylamino]ethyl]-N-methyl-, 1,1-dimethylethyl ester
CAS No.:916084-87-2
Molecular Formula:C34H59N3O7Si2
Molecular Weight:678.029
Hs Code.:

Carbamic acid,
N-[2-[[[2,6-bis[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-4-[(2-propyn-
1-ylamino)carbonyl]phenoxy]carbonyl]methylamino]ethyl]-N-methyl-,
1,1-dimethylethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, N-[2-[[[2,6-bis[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-4-[(2-propyn- 1-ylamino)carbonyl]phenoxy]carbonyl]methylamino]ethyl]-N-methyl-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Useful:

Technology Process of Carbamic acid, N-[2-[[[2,6-bis[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-4-[(2-propyn- 1-ylamino)carbonyl]phenoxy]carbonyl]methylamino]ethyl]-N-methyl-, 1,1-dimethylethyl ester

There total 6 articles about Carbamic acid, N-[2-[[[2,6-bis[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-4-[(2-propyn- 1-ylamino)carbonyl]phenoxy]carbonyl]methylamino]ethyl]-N-methyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 916084-86-1
2,6-bis((tert-butyldimethylsilyloxy)methyl)-4-(prop-2-ynylcarbamoyl)phenyl 4-nitrophenyl carbonate

: 112257-19-9
tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate

: 916084-87-2
(2-{[2,6-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-prop-2-ynylcarbamoyl-phenoxycarbonyl]-methyl-amino}-ethyl)-methyl-carbamic acid tert-butyl ester

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1002/chem.200601263 DOI:10.1016/j.bmc.2007.08.046

Reference yield:

: 916084-84-9
4-hydroxy-3,5-bis(hydroxymethyl)-N-(prop-2-ynyl)benzamide

: 916084-87-2
(2-{[2,6-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-prop-2-ynylcarbamoyl-phenoxycarbonyl]-methyl-amino}-ethyl)-methyl-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / imidazole / dimethylformamide / 2 h / 20 °C

2: 90 percent / NEt₃ / tetrahydrofuran / 1 h / 20 °C

3: 90 percent / dimethylformamide / 1 h / 20 °C

With 1H-imidazole; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601263

Reference yield:

: 916084-85-0
3,5-bis((tert-butyldimethylsilyloxy)methyl)-4-hydroxy-N-(prop-2-ynyl)benzamide

: 916084-87-2
(2-{[2,6-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-prop-2-ynylcarbamoyl-phenoxycarbonyl]-methyl-amino}-ethyl)-methyl-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NEt₃ / tetrahydrofuran / 1 h / 20 °C

2: 90 percent / dimethylformamide / 1 h / 20 °C

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/chem.200601263