1,3,8-Triazaspiro[4.5]decane-2,4-dione, 8-[(3,5-dimethoxyphenyl)methyl]-1-(2-methoxyethyl)-3-[(3,4,5-trimethoxy phenyl)methyl]-

Base Information

Chemical Name:1,3,8-Triazaspiro[4.5]decane-2,4-dione, 8-[(3,5-dimethoxyphenyl)methyl]-1-(2-methoxyethyl)-3-[(3,4,5-trimethoxy phenyl)methyl]-
CAS No.:916157-43-2
Molecular Formula:C29H39N3O8
Molecular Weight:557.644
Hs Code.:

Synonyms:

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Chemical Property of 1,3,8-Triazaspiro[4.5]decane-2,4-dione, 8-[(3,5-dimethoxyphenyl)methyl]-1-(2-methoxyethyl)-3-[(3,4,5-trimethoxy phenyl)methyl]-

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Technology Process of 1,3,8-Triazaspiro[4.5]decane-2,4-dione, 8-[(3,5-dimethoxyphenyl)methyl]-1-(2-methoxyethyl)-3-[(3,4,5-trimethoxy phenyl)methyl]-

There total 7 articles about 1,3,8-Triazaspiro[4.5]decane-2,4-dione, 8-[(3,5-dimethoxyphenyl)methyl]-1-(2-methoxyethyl)-3-[(3,4,5-trimethoxy phenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 959618-96-3
C₁₉H₂₇N₃O₅

: 3840-30-0
5-(chloromethyl)-1,2,3-trimethoxybenzene

: 916157-43-2
C₂₉H₃₉N₃O₈

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 180 ℃; for 0.0166667h; Microwave irradiation;

Reference yield:

: 959618-94-1
C₁₄H₁₉NO₃

: 916157-43-2
C₂₉H₃₉N₃O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol; water

2.1: hydrogenchloride / methanol; water / 40 °C

3.1: potassium cyanide / methanol; water / 18 h / 20 °C

4.1: dichloromethane / 1 h / 20 °C

4.2: 1.17 h / 20 - 110 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.02 h / 180 °C / Microwave

With hydrogenchloride; potassium cyanide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: C₁₇H₂₆N₂O₃

: 916157-43-2
C₂₉H₃₉N₃O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / methanol; water / 40 °C

2.1: potassium cyanide / methanol; water / 18 h / 20 °C

3.1: dichloromethane / 1 h / 20 °C

3.2: 1.17 h / 20 - 110 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.02 h / 180 °C / Microwave

With hydrogenchloride; potassium cyanide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane; water; N,N-dimethyl-formamide;