2,3-Dibromosuccinic acid, (2R,3R)-

Base Information

• Chemical Name: 2,3-Dibromosuccinic acid, (2R,3R)-
• CAS No.: 1114-00-7
• Molecular Formula: C4H4 Br2 O4
• Molecular Weight: 275.881
• European Community (EC) Number: 214-210-7
• UNII: EK5D0R9G40
• DSSTox Substance ID: DTXSID301278429
• Nikkaji Number: J238.605D
• Wikidata: Q27887888
• ChEMBL ID: CHEMBL1333362
• Mol file: 1114-00-7.mol

Synonyms:UNII-EK5D0R9G40;2,3-Dibromosuccinic acid, (2R,3R)-;EK5D0R9G40;Butanedioic acid, 2,3-dibromo-, (2R,3R)-;(+/-)-2,3-dibromosuccinic acid;916065-44-6;1114-00-7;NSC-203337;608-35-5;(2R,3R)-2,3-dibromobutanedioic acid;NCIStruc1_000909;NCIStruc2_001629;2,3-Dibromo butanedioic acid;CHEMBL1333362;DTXSID301278429;(2R,3R)-2,3-dibromosuccinic acid;CCG-36809;NCGC00014562;NCI203337;NCGC00014562-02;NCGC00097666-01;HY-133681;rel-(2R,3R)-2,3-Dibromobutanedioic acid;CS-0129001;Q27887888;( inverted exclamation markA)-2,3-Dibromosuccinic acid

Chemical Property of 2,3-Dibromosuccinic acid, (2R,3R)-

Chemical Property:

• Vapor Pressure: 0.00323mmHg at 25°C
• Boiling Point: 262.4°Cat760mmHg
• Flash Point: 112.5°C
• Density: 2.486g/cm³
• XLogP3: 1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 275.84558
• Heavy Atom Count: 10
• Complexity: 139

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(C(=O)O)Br)(C(=O)O)Br
• Isomeric SMILES: [C@H]([C@@H](C(=O)O)Br)(C(=O)O)Br

Technology Process of 2,3-Dibromosuccinic acid, (2R,3R)-

There total 25 articles about 2,3-Dibromosuccinic acid, (2R,3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(2E)-but-2-enedioic acid (110-17-8,26099-09-2) → 2,3-dibromosuccinic acid (526-78-3,608-35-5,608-36-6,1114-00-7)

Guidance literature:

With hydrogen bromide; bromine; In water; at 70 - 80 ℃; for 1h;

Reference yield:

→ meso-2,3-dibromosuccinic acid (608-36-6) + (+-)-2,3-dibromosuccinic acid (1114-00-7)

Guidance literature:

With bromine;

Reference yield:

maleic anhydride (108-31-6) → meso-2,3-dibromosuccinic acid (608-36-6) + (+-)-2,3-dibromosuccinic acid (1114-00-7)

Guidance literature:

With chloroform; bromine; im Sonnenlicht und Zersetzung des Reaktionsprodukts mit Wasser;

upstream raw materials:

(2E)-but-2-enedioic acid

1,2-Dibromosuccinic anhydride

water

(2R,3R)-2,3-diaminosuccinic acid

Downstream raw materials:

cis-2-bromobutenedioic acid

(2E)-but-2-enedioic acid

racem-2,3-bis-benzylamino-succinic acid

N,N'-dibenzyltartramide

Refernces

• 1、 Erickson,L.E.. "-". . p. 1867 - 1875. Retrieved 1965.
• 2、 -. "Synthesis method of o-Dibromo compound". Paragraph 0060-0067. . Retrieved 2022/01/04.
• 3、 -. "Preparation method of 1,3-dibenzyl-2-oxoimidazolidine-4,5-dicarboxylic acid". Paragraph 0046; 0047; 0054; 0055; 0058-0063. . Retrieved 2017/08/30.