1-BENZYL-4-NITROSOPIPERAZINE

Base Information

• Chemical Name: 1-BENZYL-4-NITROSOPIPERAZINE
• CAS No.: 40675-45-4
• Molecular Formula: C11H15 N3 O
• Molecular Weight: 205.26
• Hs Code.: 2933599090
• Mol file: 40675-45-4.mol

Synonyms:Piperazine,1-benzyl-4-nitoso- (5CI); 1-Benzyl-4-nitrosopiperazine

Chemical Property of 1-BENZYL-4-NITROSOPIPERAZINE

Chemical Property:

• Vapor Pressure: 4.35E-05mmHg at 25°C
• Melting Point: 56-58°C
• Boiling Point: 350.6°Cat760mmHg
• Flash Point: 165.8°C
• PSA: 35.91000
• Density: 1.16g/cm³
• LogP: 1.36140
• Storage Temp.: -20°C Freezer

Purity/Quality:

99% ^*data from raw suppliers

1-Benzyl-4-nitrosopiperazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-BENZYL-4-NITROSOPIPERAZINE

There total 3 articles about 1-BENZYL-4-NITROSOPIPERAZINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.3%

1-phenylmethylpiperazine (2759-28-6) → 1-benzyl-4-nitroso-4-piperizine (40675-45-4)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; at 0 - 20 ℃;

Reference yield:

N-nitrosopiperazine (5632-47-3) + benzyl bromide (100-39-0) → 1-benzyl-4-nitroso-4-piperizine (40675-45-4)

Guidance literature:

With triethylamine; In acetonitrile; for 3h; Heating;

DOI:10.1021/jm050498l

Reference yield:

→ 1-benzyl-4-nitroso-4-piperizine (40675-45-4)

Guidance literature:

N-Benzyl-piperazin, NaNO2, HCl, (75grad);

upstream raw materials:

1-phenylmethylpiperazine

N-nitrosopiperazine

benzyl bromide

Downstream raw materials:

4-benzylpiperazin-1-amine

1-benzyl[3,3,5,5-2H₄]piperazine

C₂₄H₂₂F₆N₆O

pentadecanoic acid (4-benzyl-piperazin-1-yl)-amide

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