Benzeneacetaldehyde, a-methoxy-a-methyl-, (R)-

Base Information

Chemical Name:Benzeneacetaldehyde, a-methoxy-a-methyl-, (R)-
CAS No.:91899-79-5
Molecular Formula:C10H12O2
Molecular Weight:164.204
Hs Code.:

Synonyms:

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Chemical Property of Benzeneacetaldehyde, a-methoxy-a-methyl-, (R)-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzeneacetaldehyde, a-methoxy-a-methyl-, (R)-

There total 10 articles about Benzeneacetaldehyde, a-methoxy-a-methyl-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 682351-19-5
((R)-1,2,2-Trimethoxy-1-methyl-ethyl)-benzene

: 91899-79-5
(S)-2-methoxy-2-phenylpropanal

Guidance literature:: With sulfuric acid; In tetrahydrofuran; for 5h; Heating;
DOI:10.1055/s-2004-815406

Reference yield:

: 1517-69-7
(R)-1-phenylethanol

: 91899-79-5
(S)-2-methoxy-2-phenylpropanal

Guidance literature:: Multi-step reaction with 7 steps

1.1: Et₃N / tetrahydrofuran / 3 h / 20 °C

2.1: NaOH; Ca(OH)2 / cetyltrimethylammonium chloride / CHCl₃ / 1 h / 20 - 50 °C / ultrasound irradiation

2.2: 135 mg / aq. HCl / methanol / 2 h / 20 °C

3.1: K₂CO₃ / methanol / 0.17 h / 20 °C

4.1: 76 percent / tetrahydrofuran / 10 h / 20 °C

5.1: 95 percent / K₂CO₃ / 10 h / 20 °C

6.1: 95 percent / NaH / dimethylformamide / 10 h / 20 °C

7.1: 75 percent / aq. H₂SO₄ / tetrahydrofuran / 5 h / Heating

With calcium hydroxide; sodium hydroxide; sulfuric acid; sodium hydride; potassium carbonate; triethylamine; cetyltrimethylammonium chloride; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-815406

Reference yield:

: 98857-41-1
(R)-(+)-1-trimethylsiloxyethylbenzene

: 91899-79-5
(S)-2-methoxy-2-phenylpropanal

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaOH; Ca(OH)2 / cetyltrimethylammonium chloride / CHCl₃ / 1 h / 20 - 50 °C / ultrasound irradiation

1.2: 135 mg / aq. HCl / methanol / 2 h / 20 °C

2.1: K₂CO₃ / methanol / 0.17 h / 20 °C

3.1: 76 percent / tetrahydrofuran / 10 h / 20 °C

4.1: 95 percent / K₂CO₃ / 10 h / 20 °C

5.1: 95 percent / NaH / dimethylformamide / 10 h / 20 °C

6.1: 75 percent / aq. H₂SO₄ / tetrahydrofuran / 5 h / Heating

With calcium hydroxide; sodium hydroxide; sulfuric acid; sodium hydride; potassium carbonate; cetyltrimethylammonium chloride; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-815406