L-Proline, 1-(2,2-dimethyl-1-oxopropyl)-, 2-carboxyphenyl ester

Base Information

Chemical Name:L-Proline, 1-(2,2-dimethyl-1-oxopropyl)-, 2-carboxyphenyl ester
CAS No.:92010-30-5
Molecular Formula:C17H21NO5
Molecular Weight:319.357
Hs Code.:

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Chemical Property of L-Proline, 1-(2,2-dimethyl-1-oxopropyl)-, 2-carboxyphenyl ester

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Technology Process of L-Proline, 1-(2,2-dimethyl-1-oxopropyl)-, 2-carboxyphenyl ester

There total 6 articles about L-Proline, 1-(2,2-dimethyl-1-oxopropyl)-, 2-carboxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 92010-29-2
(S)-1-(2,2-Dimethyl-propionyl)-pyrrolidine-2-carboxylic acid 2-benzyloxycarbonyl-phenyl ester

: 92010-30-5
(S)-1-(2,2-Dimethyl-propionyl)-pyrrolidine-2-carboxylic acid 2-carboxy-phenyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; under 1551.4 Torr;
DOI:10.1021/jm00378a005

Reference yield:

: 118-58-1
benzyl salicylate

: 92010-30-5
(S)-1-(2,2-Dimethyl-propionyl)-pyrrolidine-2-carboxylic acid 2-carboxy-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / DMAP, DCC / CH₂Cl₂ / 18 h

2: 51 percent / H₂ / 10percent Pd/C / methanol / 3 h / 1551.4 Torr

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00378a005

Reference yield:

: 16652-71-4
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride

: 92010-30-5
(S)-1-(2,2-Dimethyl-propionyl)-pyrrolidine-2-carboxylic acid 2-carboxy-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / DMAP, DCC / CH₂Cl₂ / Ambient temperature

2: 55 percent / H₂ / 10percent Pd/C / methanol / 3 h / 1551.4 Torr

3: 64 percent / DMAP, DCC / CH₂Cl₂ / 18 h

4: 51 percent / H₂ / 10percent Pd/C / methanol / 3 h / 1551.4 Torr

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00378a005