Glycine, N-(2-ethoxy-2-oxoethyl)-N-[2-(3-hydroxypropoxy)phenyl]-, ethyl ester

Base Information

Chemical Name:Glycine, N-(2-ethoxy-2-oxoethyl)-N-[2-(3-hydroxypropoxy)phenyl]-, ethyl ester
CAS No.:920268-19-5
Molecular Formula:C17H25NO6
Molecular Weight:339.389
Hs Code.:

Synonyms:{Ethoxycarbonylmethyl-[2-(3-hydroxy-propoxy)-phenyl]-amino}-acetic acid ethyl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Glycine, N-(2-ethoxy-2-oxoethyl)-N-[2-(3-hydroxypropoxy)phenyl]-, ethyl ester

Chemical Property:

Boiling Point:449.9±40.0 °C(Predicted)
PSA：85.30000
Density:1.178±0.06 g/cm3(Predicted)
LogP:1.38040

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Glycine, N-(2-ethoxy-2-oxoethyl)-N-[2-(3-hydroxypropoxy)phenyl]-, ethyl ester

There total 2 articles about Glycine, N-(2-ethoxy-2-oxoethyl)-N-[2-(3-hydroxypropoxy)phenyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 920268-18-4
3-(2-aminophenoxy)propan-1-ol

: 105-36-2
ethyl bromoacetate

: 920268-19-5
diethyl 2,2'-(2-(3-hydroxypropoxy)phenylazanediyl)diethanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; sodium iodide; In N,N-dimethyl-formamide; at 100 ℃; for 30h;
DOI:10.1021/ja065264l

Reference yield:

: 38340-87-3
3-(2-nitrophenoxy)propan-1-ol

: 920268-19-5
diethyl 2,2'-(2-(3-hydroxypropoxy)phenylazanediyl)diethanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / ethanol; ethyl acetate / 48 h / 20 °C / 760 Torr

2: 87 percent / NaI; iPr₂NEt / dimethylformamide / 30 h / 100 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In ethanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja065264l

Reference yield:

: 920268-19-5
diethyl 2,2'-(2-(3-hydroxypropoxy)phenylazanediyl)diethanoate

: 920268-21-9
diethyl 2,2'-(2-(3-(1,4,7,10-tetraazacyclododec-1-yl)propoxy)phenylazanediyl)diethanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / CBr₄; Ph₃P / CH₂Cl₂ / 3 h / 0 °C

2: 85 percent / CHCl₃ / 48 h / 20 °C

With carbon tetrabromide; triphenylphosphine; In dichloromethane; chloroform;
DOI:10.1021/ja065264l