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8-Dodecenoic acid, 11-(benzoyloxy)-, (E)-

Base Information
  • Chemical Name:8-Dodecenoic acid, 11-(benzoyloxy)-, (E)-
  • CAS No.:92051-74-6
  • Molecular Formula:C19H26O4
  • Molecular Weight:318.413
  • Hs Code.:
8-Dodecenoic acid, 11-(benzoyloxy)-, (E)-

Synonyms:

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Chemical Property of 8-Dodecenoic acid, 11-(benzoyloxy)-, (E)-
Chemical Property:
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Technology Process of 8-Dodecenoic acid, 11-(benzoyloxy)-, (E)-

There total 9 articles about 8-Dodecenoic acid, 11-(benzoyloxy)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 9 steps
1: 1.) LiNH2, liq. NH3
2: 85 percent / NaNH2, 1,3-diaminopropane / 2.5 h / 80 °C
3: 85 percent / PTSA / CH2Cl2
4: 65 percent / n-BuLi, BF3*Et2O / tetrahydrofuran; hexane / -78 °C
5: 90 percent / Na/liq. NH3 / tetrahydrofuran / 4 h / -33 °C
6: 87 percent / pyridine
7: 85 percent / PTSA / ethanol
8: 67 percent / pyridinium dichromate / CH2Cl2 / 6 h / Ambient temperature
9: aq. silver nitrate, KOH / ethanol / 24 h / Ambient temperature
With pyridine; potassium hydroxide; dipyridinium dichromate; n-butyllithium; lithium amide; boron trifluoride diethyl etherate; ammonia; sodium; toluene-4-sulfonic acid; sodium amide; silver nitrate; Trimethylenediamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;
Guidance literature:
Multi-step reaction with 6 steps
1: 65 percent / n-BuLi, BF3*Et2O / tetrahydrofuran; hexane / -78 °C
2: 90 percent / Na/liq. NH3 / tetrahydrofuran / 4 h / -33 °C
3: 87 percent / pyridine
4: 85 percent / PTSA / ethanol
5: 67 percent / pyridinium dichromate / CH2Cl2 / 6 h / Ambient temperature
6: aq. silver nitrate, KOH / ethanol / 24 h / Ambient temperature
With pyridine; potassium hydroxide; dipyridinium dichromate; n-butyllithium; boron trifluoride diethyl etherate; ammonia; sodium; toluene-4-sulfonic acid; silver nitrate; In tetrahydrofuran; ethanol; hexane; dichloromethane;
Guidance literature:
Multi-step reaction with 8 steps
1: 85 percent / NaNH2, 1,3-diaminopropane / 2.5 h / 80 °C
2: 85 percent / PTSA / CH2Cl2
3: 65 percent / n-BuLi, BF3*Et2O / tetrahydrofuran; hexane / -78 °C
4: 90 percent / Na/liq. NH3 / tetrahydrofuran / 4 h / -33 °C
5: 87 percent / pyridine
6: 85 percent / PTSA / ethanol
7: 67 percent / pyridinium dichromate / CH2Cl2 / 6 h / Ambient temperature
8: aq. silver nitrate, KOH / ethanol / 24 h / Ambient temperature
With pyridine; potassium hydroxide; dipyridinium dichromate; n-butyllithium; boron trifluoride diethyl etherate; ammonia; sodium; toluene-4-sulfonic acid; sodium amide; silver nitrate; Trimethylenediamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;
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