1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthylamine

Base Information

Chemical Name:1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthylamine
CAS No.:21489-50-9
Molecular Formula:C12H17NO2
Molecular Weight:207.272
Hs Code.:2922299090
DSSTox Substance ID:DTXSID10944082
Nikkaji Number:J42.467F
Mol file:21489-50-9.mol

Synonyms:1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthylamine;21489-50-9;5,6-dimethoxy-1,2,3,4-tetrahydronaphthalen-2-amine;beta-Naphthylamine, 5,6-dimethoxy-1,2,3,4-tetrahydro-;5,6-Dimethoxy-1,2,3,4-tetrahydro-beta-naphthylamine;2-NAPHTHYLAMINE, 1,2,3,4-TETRAHYDRO-5,6-DIMETHOXY-;1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthalenamine;SCHEMBL6546842;5,6-dimethoxy-2-amino-tetralin;DTXSID10944082;BDHOUGWYKHSPIX-UHFFFAOYSA-N;LS-95802;PD033611;FT-0765903;1,2,3,4-tetrahydro-5,6-dimethoxy-2- aminonaphthalene

Suppliers and Price of 1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5,6-DIMETHOXY-2-AMINOTETRALIN 95.00%
5MG
$ 501.64

Total 2 raw suppliers

Chemical Property of 1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthylamine

Chemical Property:

Vapor Pressure:9.42E-05mmHg at 25°C
Boiling Point:339.1°Cat760mmHg
Flash Point:174.1°C
PSA：44.48000
Density:1.08g/cm³
LogP:2.22010
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:207.125928785
Heavy Atom Count:15
Complexity:210

Purity/Quality:

95% ^*data from raw suppliers

5,6-DIMETHOXY-2-AMINOTETRALIN 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C2=C(CC(CC2)N)C=C1)OC

Technology Process of 1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthylamine

There total 10 articles about 1,2,3,4-Tetrahydro-5,6-dimethoxy-2-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 885058-67-3
phenylmethyl (1,2,3,4-tetrahydro-5,6-dimethoxynaphthalen-2-yl)carbamate

: 21489-50-9
5,6-dimethoxy-2-aminotetrahydronaphthalene

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; chloroform; at 20 ℃; for 24h;
DOI:10.1002/hlca.200690030

Reference yield:

: 885058-66-2
1,2,3,4-tetrahydro-5,6-dimethoxynaphthalene-2-carboxylic acid

: 21489-50-9
5,6-dimethoxy-2-aminotetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: diphenylphosphoryl azide; Et₃N / benzene / 6 h / Heating

2: benzene / 30 h / Heating

3: 95 percent / H₂ / Pd/C / CHCl₃; methanol / 24 h / 20 °C

With diphenylphosphoranyl azide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform; benzene; 1: Curtius rearrangement;
DOI:10.1002/hlca.200690030

Reference yield:

: (5,6-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-carbamic acid

: 21489-50-9
5,6-dimethoxy-2-aminotetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 30 h / Heating

2: 95 percent / H₂ / Pd/C / CHCl₃; methanol / 24 h / 20 °C

With hydrogen; palladium on activated charcoal; In methanol; chloroform; benzene;
DOI:10.1002/hlca.200690030